silica sulfuric acid is employed as solid acid catalyst for the clean and less hazardousprotection of carbonyl compounds as 2,4-dinitrophenylhydrazone under solvent-free conditions.

sulfuric acid ([3-(3-silicapropyl)sulfanyl]propyl]ester (saspspe) is employed as a recyclable catalyst for the silylation of hydroxyl groups. a good range of primary, secondary alcohols and phenolic hydroxyl groups were effectively converted into their corresponding trimethylsilyl ethers with hexamethyldisilazane in the presence of catalytic amounts of saspspe at room temperature with short rea...

SnCl4/nano-sawdust was prepared as a carbohydrate-based catalyst containing of tin bearing cellulose units. The catalyst was characterized by X-ray diffraction (XRD), fourier transform infrared spectroscopy (FT-IR), field emission scanning electron microscopy (FESEM) and energy dispersive X-ray spectroscopy (EDS). The catalyst was applied successfully as a readily available, inexpensive, biodeg...

cofe2o4 magnetic nanoparticles were modified by dopamine (da) and ascorbic acid (aa) as anchors. separation of the da and aa using cofe2o4 magnetic nanoparticles have been studied by investigating the effects of ph, concentration of the da and aa, amount of adsorbents, contact time, ionic strength and temperature. the mechanism of adsorption was also studied. the adsorption of da and aa to the ...

sulfonic acid functionalized sba-15 (sba-pr-so3h) as a new nanoporous acid catalyst was used in the one-pot synthesis of polyhydroquinolines derivatives via the hantzsch four component condensation reaction of aldehydes, b-ketoesters, dimedone and ammonium acetate under solvent free conditions with short reaction time in excellent yields. sba-pr-so3h was proved to be an efficient heterogeneous ...

easily synthesized1-methyl-3-(2-oxyethyl)-1h-imidazol-3-ium-borate sulfonic acid {[moei]-bsa} as a novel catalyst efficiently promoted the synthesis of quinoxaline derivatives via condensation of various diamines with 1,2-dicarbonyl compounds at room temperature conditions in ethanol. this research provides a new method for the synthesis of quinoxalines in good to excellent yields with little c...

A novel, rapid and simple method is described for the synthesis of magnetic MIL-100(Fe) with novel Fe3O4 morphology, which significantly improved the sustainability of conventional fabrication processes in several aspects. The magnetic MOFs were prepared (i) in one pot (instead of multiple steps), (ii) at room temperature (instead of temperatures over 150 °C), (iii) within a few hours with exce...

Nano silica sulfuric acid as a solid acid, was described to be an effective catalyst for one-pot three-component reaction of kojic acid, aryl aldehydes and indoles for the preparation of 2-substituted aryl (indolyl) kojic acid derivatives. The catalyst was prepared by combination of chlorosulfonic acid to nano silica gel. The size of nanoparticles were observed with SEM.All prepared compounds w...

A series of arylidine barbituric acid derivatives was synthesized by Knoevenagel condensation reaction of aromatic aldehydes with barbituric acid or thiobarbituric acid using dodecylbenzenesulfonic acid as a Brønsted acid-surfactant catalyst in aqueous media. Regardless of the nature of the substitution (electron-donating and -withdrawing), all the reactions were completed within 15-65 min in w...

The photocatalytic degradation of organic compounds of olive mill wastewater (OMWW) was investigated by using core-shell-shell Fe3O4/SiO2/TiO2 nanoparticles as catalyst. The preparation of nanoparticles was performed by coating onto magnetic nanoparticles a SiO2 layer, using Stober method and TiO2 layer, using sol-gel method. The photo catalyst was characterized by dynamic light scattering (DLS...