نتایج جستجو برای: microwave assisted method
تعداد نتایج: 1780692 فیلتر نتایج به سال:
The aim of this work is to compare the extraction efficiencies of microwave and conventional isolation of mangiferin from Mangifera indica L. The parameters studied, which might affect the extraction efficiency were extraction time, solvent composition and microwave power. The conventional heating 21 h provided 5.23 % yield of mangiferin and by microwave heating at 210 W for 56 min, the yield w...
The aim of present study was to compare the effects of ultrasound-assisted and microwave-assisted extraction with solvent extraction method on antioxidant activities of jujube (Ziziphus mauritiana Lam.) leaf extracts in stability of sunflower oil during deep frying. The antioxidant activities of the extracts were evaluated by using 2, 2-diphenyl-1-picrylhydrazyl (DPPH˙) radical scavenging and β...
Microwave-assisted pyrolysis of seaweed biomass was conducted using a microwave system. The product yields were determined and the components bio-oil analyzed by gas chromatography-mass spectrometry (GC-MS). Results showed that as temperature increased from 400 °C to 600 °C, yield bio-char decreased. However, rose firstly then reduced. maximal 18.4 wt.% when 500 °C. obtained is mixture very com...
ZnO nanorod was prepared by microwave assisted method. The crystal structure of the nano powders were confirmed by X-Ray diffraction analysis and the mean particle size was estimated by the Scherrer,s formula .The surface morphology of the nano particles were analyzed by using SEM . The absorption spectrum of the material in the UV-Vis range was recorded .The energy band gap of the...
ZnO nanorod was prepared by microwave assisted method. The crystal structure of the nano powders were confirmed by X-Ray diffraction analysis and the mean particle size was estimated by the Scherrer,s formula .The surface morphology of the nano particles were analyzed by using SEM . The absorption spectrum of the material in the UV-Vis range was recorded .The energy band gap of the...
This paper outlines the synthesis of CuFe2O4 nanoparticles and their catalytic applications. CuFe2O4 nanoparticles were synthesized via microwave-assisted co-precipitation method. The obtained nanoparticles characterized through Fourier transform infrared spectroscopy, X-ray diffraction, and scanning electron microscopy. Vibrating sample magnetometer shows nanoparticles exhibit ferromagnetic be...
Ultra-fast and large-quantity (grams) synthesis of one-dimensional ZnO nanowires has been carried out by a novel microwave-assisted method. High purity Zinc (Zn) metal was used as source material and placed on microwave absorber. The evaporation/oxidation process occurs under exposure to microwave in less than 100 s. Field effect scanning electron microscopy analysis reveals the formation of hi...
The present paper describes studies on the synthesis of the antiepileptic drug phenytoin, and of structurally related derivatives. First, the influence of the solvent has been investigated in the microwave-assisted synthesis of the drug, resulting in a yield improvement and a cleaner reaction. Second, a two-step reaction is described to synthesize selectively and in high yields phenytoin. The f...
This work reports a novel approach where three phase partitioning (TPP) was combined with microwave for extraction of mangiferin from leaves of Mangifera indica. Soxhlet extraction was used as reference method, which yielded 57 mg/g in 5 h. Under optimal conditions such as microwave irradiation time 5 min, ammonium sulphate concentration 40% w/v, power 272 W, solute to solvent ratio 1:20, slurr...
Plant extracts having an inhibitory effect on aging may be a good choice for cosmetic applications because of their natural origin. The extraction of bioactive compounds from plants is one of the most critical steps in the commercial development of natural products. Therefore rapid and efficient phytochemical extraction methods are essential. The present study involves the use of microwave and ...
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