A co-precipitation method was used for synthesis of pure MgTiO3 ceramic powder with Mg(NO3)2.6H2O, TiCl4 or C12H28O4Ti and NaOH as raw materials. In this method, solutions of 1 M, Mg (NO3)2 6H2O and 2 M, NaOH were prepared. A stoichiometric amount of Ti precursors from TiCl4 or C12H28O4Ti was weighted. Solutions of Mg (NO3)2. 6H2O and Ti precursor were added dropwise to NaOH solution unde...

A computer model for the sintering of ceramic/polymer composite materials has been established based on empirical sintering rate data. The model calculates sintering depths which result from variations in the operating parameters which include laser power, beam speed, scan spacing, scan vector length, and initial temperatures of the powder and surroundings. Sintering depths measured in multiple...

Lightweight corundum-mullite thermal insulation materials were successfully prepared by microwave sintering at low temperature. The effects of temperatures, PMMA microspheres and SiC particles on structure properties as-prepared investigated. became a hot spot under the action field, these local high temperature areas promoted formation growth mullite whiskers. burn out, leaving pores which cou...

In the present study, controllable microwave sintering was applied to prepare partially stabilised zirconia ceramics with enhanced phase composition and a more uniform structure. To reveal interface properties structural changes of PSZ during process, XRD, FT-IR, Raman, SEM characterisations were utilised. XRD analysis Raman demonstrated that increase temperature promoted martensite conversion....

We present fast sintering for silver (Ag) nanoparticle (NP) and flake layers printed using roll-to-roll (R2R) gravure printing. An infrared (IR) sintering module was applied to an R2R system to shorten the sintering duration of an R2R gravure-printed Ag layer. IR sintering of the conductive layer was improved by optimising the process condition. After printing of the Ag NP and Ag flake layers, ...

This paper describes thermoelectric properties of La-doped SrTiO3 prepared by using a combination of combustion synthesis (CS) with post spark plasma sintering (SPS), on which effects of sintering temperature were mainly examined. In experimental, combustion-synthesized (CSed) samples (Sr1 xLaxTiO3, x 1⁄4 0:08) were spark-plasma-sintered (SPSed) at temperatures from 1513 to 1663K and the thermo...

the fuel cells are distinguished as generating of green allocable energy and are electrochemical devices of low environmental impact. porous nanocrystalline strontium-doped lanthanum manganite la0.8sr0.2mno3 (lsm) cathode materials were prepared by mechanochemical route in various grinding times. carbon black was employed to produce pores. the formation of lsm single phase was studied by x-ray ...

Sintering with low frequency rf power (-50 M H z ) is a new technique with unique capabilities that has been used to sinter a variety of ceramic materials, including zirconia-toughened alumina, alumina, silicon carbide, and boron carbide. Processing with low frequencies offers many advantages compared to processing with conventional microwave frequencies (915 MHz and 2.45 GHz). Because of the l...

In the present paper the sintering behavior of 3 mol% yttria-stabilized zirconia (3Y-TZP) with and without small amount (0.2 wt %) of SiO2 additive was investigated. It has been studied the silica impact which was added in two ways (co-precipitation and mechanical mixing) on sintering kinetics of 3Y-TZP nanopowders at the initial sintering stage. It was found the silica additive leads to the ch...