synthesis of bafe12o19 magnetic nano particles via precipitation in different ph conditions have been reported. the certain molar ratio of fe/ba = 12 selected and sodium hydroxide was used as a precipitant agent. x-ray diffraction (xrd), scanning electron microscopy (sem) and vibrating sample magnetometer (vsm) were used to consider the structural, morphological and magnetic properties of bariu...

Well shaped single crystalline Mn3O4 nano-octahedra with exposed highly active {011} facets at different particle sizes have been synthesized and used as anode materials for lithium ion batteries. The electrochemical results show that the smallest sized Mn3O4 nano-octahedra show the best cycling performance with a high initial charge capacity of 907 mA h g(-1) and a 50th charge capacity of 500 ...

The structural analysis of the synthetic glycolipid crystalline phase has been performed during the past few decades; however, it has not been sufficiently understood in terms of both static and dynamic aspects. We have recently shown that grazing incidence X-ray diffraction (GIXD) affords better information than conventional powder X-ray diffraction (PXRD) for the crystal structure analysis of...

The mechanical behavior of bicrystalline aluminum nano-pillars under uniaxial compression reveals size effects, a stochastic stress– strain signature, and strain hardening. Pillar diameters range from 400 nm to 2 lm and contain a single, non-sigma high angle grain boundary oriented parallel to the pillar axes. Our results indicate that these bicrystalline pillars are characterized by intermitte...

A comparison has been drawn in pure anatase and rutile forms of TiO2 films with their respective nano crystalline forms as photoanodes in dye-sensitized solar cells. All the films have been synthesized by using sol-gel method. Crystalline nature of the films has been investigated by x-ray diffraction (XRD) and morphologies have been studied by scanning electron microscopy (SEM). The short-circu...

Nano-silicon is a nanostructured material in which quantum or spatial confinement is the origin of the material's luminescence. When nano-silicon is broken into colloidal crystalline nanoparticles, its luminescence can be tuned across the visible spectrum only when the sizes of the nanoparticles, which are obtained via painstaking filtration methods that are difficult to scale up because of low...

Whilst the use of microscopic techniques to determine the size distributions of nanoparticle samples is now well established, their characterisation challenges extend well beyond this. Here it is shown how high resolution electron microscopy can help meet these challenges. One of the key parameters is the determination of particle shape and structure in three dimensions. Here two approaches to ...

Bacterial cellulose is a biological polymer with a variety of extraordinary properties which make it a functional material for different industrial fields. This work aimed at monitoring the effects of three different organic acids and nanoparticles on the production, water holding capacity and structural characteristics of bacterial cellulose. Different concentrations of organic acids and nanop...