Abstract Organotin compounds are widely employed as pesticides and fungicides in agriculture stabilizers for the industrial manufacture of polyvinyl chloride other polymers. Accordingly, these endocrine disruptors can be found a variety foods beverages. In present study, we describe optimization hollow-fiber liquid-phase micro-extraction approach simultaneous derivatization, extraction, pre-con...

abstract: a combined gas chromatography-mass spectrometry (gc-ms) with headspace solid-phase micro extraction (spme) method has been employed for the analysis of the flavor volatiles of three different rice cultivar, including two modified iranian rice cultivars and hashemi rice cultivar during gelatinization. the proposed combination provided a powerful system for easy and rapid screening of a...

a comprehensive study pertaining to the emulsion liquid membrane (elm) extraction process to enrich dilute aqueous solutions of silver salt is presented. the study has highlighted the importance and influence of membrane composition for maximizing the extraction of ag+ ions. the liquid membrane was made up of cyanex-302 as an extractant and the industrial solvent mainly consists of paraffinic a...

We present parallel processing implementation for rapid extraction of the quantitative phase maps from off-axis holograms on the Graphics Processing Unit (GPU) of the computer using computer unified device architecture (CUDA) programming. To obtain efficient implementation, we parallelized both the wrapped phase map extraction algorithm and the two-dimensional phase unwrapping algorithm. In con...

In this study, we performed micro-scale dynamic laminar flow extraction and site-specific in situ chloride concentration measurements. Surface-enhanced Raman spectroscopy was utilized to investigate the diffusion process of chloride ions from an oil phase to a water phase under laminar flow. In contrast to common logic, we used SERS intensity gradients of Rhodamine 6G to quantitatively calculat...

For DNA purification to be functionally integrated into the microchip for high-throughput DNA analysis, a miniaturized purification process must be developed that can be easily adapted to the microchip format. In this study, we evaluate the effectiveness of a variety of silica resins for miniaturized DNA purification and gauge the potential usefulness for on-chip solid-phase extraction. A micro...

Present study aims the optimisation and validation of the extraction procedures for the determination of polycyclic aromatic hydrocarbons (PAHs) in sediment samples. As analytical techniques, gas chromatographymass detector (GC-MS) and gas chromatography-flame ionization detector (GC-FID). The optimized methods were soxhlet extraction, ultrasonic bath extraction and solid phase micro extraction...

Spectrometric techniques for the analysis of trace cadmium have developed rapidly due to the increasing need for accurate measurements at extremely low levels of this element in diverse matrices. This review covers separation and preconcentration procedures, such as electrochemical deposition, precipitation, coprecipitation, solid phase extraction, liquid-liquid extraction (LLE) and cloud point...

background: bisphenol a (bpa) is one of the hazardous materials causing disruption of endocrine pathways. due to water contamination by this component from multiple sources and the associated health problems, bpa has been the focus of multiple studies. it has been proved that bpa may cause harm because of its impact on estrogenic receptors in human and other organisms. methods: in this study, t...