Field Emission Scanning Electron Microscopy (FESEM) demonstrates spectacular changes in the morphology of thin films of copper (II) phthalocyanine (CuPc) deposited on gold coated quartz substrates at different substrate temperatures, and on indium tin oxide (ITO) substrates at room temperature followed by post deposition annealing at various temperatures under normal atmosphere. The nature of s...

Zn1 - x Mn x O nanoparticles have been synthesized by hydrothermal technique. The doping concentration of Mn can reach up to 9 at% without precipitation or secondary phase, confirmed by electron spin resonance (ESR) and synchrotron X-ray diffraction (XRD). Room-temperature ferromagnetism is observed in the as-prepared nanoparticles. However, the room-temperature ferromagnetism disappears after ...

Nitrogen-doped carbon nanoparticles were synthesized via a solution plasma process, with acrylonitrile as a single-source precursor, followed by a post-thermal annealing process. The nitrogen-bonding states can be tuned by varying the annealing temperature. The best electrocatalytic activity for oxygen reduction reaction (ORR) in terms of both onset potential and limiting current density can be...

Evolution of microstructure morphologies and grain orientations of Cu-Cu bonded wafers during bonding and annealing were studied by means of transmission electron microscopy, electron diffraction and X-ray diffraction. The bonded Cu grain structure reaches steady state after post-bonding anneal. An abnormal (220) grain growth was observed during the initial bonding process. Upon annealing, the ...

The changes in the mechanical properties and microstructure of nanocrystalline Cu-Zn alloys deformed by cryorolling during low temperature annealing and the post-process deformation were studied. The deformed Cu-Zn alloys exhibited uncommon anneal hardening and deformation softening behaviors. The degree of anneal hardening and deformation softening increased with the addition of the solute ato...

This paper provides an introduction in the field of severe plastic deformation (SPD). First of all the main methods to produce SPD materials are discussed. In the following section, the mechanisms leading to the formation of fine grains are reviewed and the influence of changes in strain path is highlighted. During post-SPD thermal annealing, some typical microstructural changes take place. The...

Two-dimensional Zinc sulfide (ZnS) nanobowl arrays were synthesized via self-assembled monolayer polystyrene sphere template floating on precursor solution surface. A facile approach was proposed to investigate the morphology evolution of nanobowl arrays by post-annealing procedure. Photoluminescence (PL) measurement of as-grown nanoarrays shows that the spectrum mainly includes two parts: a pu...

We performed optical annealing experiments at the edges of nanopatterned graphene to study the resultant edge reconstruction. The lithographic patterning direction was orthogonal to a zigzag edge. μ-Raman spectroscopy shows an increase in the polarization contrast of the G band as a function of annealing time. Furthermore, transport measurements reveal a 50% increase of the GNR energy gap after...