Herein, we report a portable electrochemical biosensor based on butyrylcholinesterase (BChE) immobilized on carbon black (CB)-modified screen-printed electrodes (SPEs) for the detection of organophosphorous pesticides in olive oil. The BChE/CB-SPE biosensor was developed to detect paraoxon in standard solutions as well as in olive oil samples previously treated with the QuEChERS method to extra...

Patulin (PAT) is a mycotoxin produced in fruits, especially apples, by diverse fungal species that can be transferred into industrial apple juice during processing. An accurate, effective, and selective method has been validated for the quantification of PAT different commercial juices combining modified µ-QuEChERS procedure with high-pressure liquid chromatography (LC) equipped triple quadrupo...

A new UHPLC-MS/MS (ultra high performance liquid chromatography coupled to tandem mass spectrometry) method was developed and validated to detect 38 anthelmintic drug residues, consisting of benzimidazoles, avermectins and flukicides. A modified QuEChERS-type extraction method was developed with an added concentration step to detect most of the analytes at <1 microg kg(-1) levels in milk. Anthe...

background: the present study was the first attempt for determination and measurement of pesticide residues in tomatoes used in salad production plants in isfahan, central iran. methods: a multiresidue method based on modified quechers (quick, easy, cheap, effective, rugged and safe) sample preparation, followed by gas chromatography mass spectrometry (gc–ms) was developed and validated for the...