The aim of this study was to synthesize a new oxetan-phenyltetrahydropyridazine-3,6-dione derivative (compound 6) using with different techniques. The first method was achieved by the preparation of a phenylhydrazine derivative (2) using three components system (3,17-aldol-estradiol, phenylhydrazine, 5-hexyn-3-ol) in presence of Copper(II). Then, 2 Was reacted with tert-butyldimethylsilyl chlor...

In this study, different derivative spectrophotometric methods are proposed for the simultaneous determination of chlorpheniramine maleate (CP), phenylephrine HCl (PE) and phenylpropanolamine HCl (PP) in their ternary mixtures and in pharmaceutical dosage forms. Spectra of single component and ternary mixtures of various concentrations and combinations from zero- to fourth-derivation were obtai...

In this study, different derivative spectrophotometric methods are proposed for the simultaneous determination of chlorpheniramine maleate (CP), phenylephrine HCl (PE) and phenylpropanolamine HCl (PP) in their ternary mixtures and in pharmaceutical dosage forms. Spectra of single component and ternary mixtures of various concentrations and combinations from zero- to fourth-derivation were obtai...

In this paper, we introduce the magnitude, orientation, and anisotropic ratio for the higher order derivative ∇k+1u (with k ≥ 1) of a function u to characterize its anisotropic behavior. The magnitude is equivalent to its usual Euclidean norm. The orientation is the direction along which the absolute value of the k + 1-th directional derivative is about the smallest, while along its perpendicul...

the present study aims at indicating the existence and uniqueness result of system in extended colombeaualgebra. the caputo fractional derivative is used for solving the system of odes. in addition, rieszfractional derivative of colombeau generalized algebra is considered. the purpose of introducing rieszfractional derivative is regularizing it in colombeau sense. we also give a solution to a n...

We explain the main techniques for estimating derivatives by simulation and survey the most recent developments in that area. In particular, we discuss perturbation analysis (PA), likelihood ratios (LR), weak derivatives (WD), nite diierences (FD), and many of their variants. We also mention some other approaches. Our discussion emphasizes the relationships between the methods. For that purpose...

The significant spectral overlap (Di) 0.5 = 0.5667 which is about 75.3% overlapping of the UV/Visible absorption spectra of iron (II) and copper (II) complexes necessitates chemometric assisted methods for simultaneous analysis of these ions in the pharmaceutical mixture. These metal ions were analyzed simultaneously by UV/Visible spectrophotometric method where 8-hydroxyquinoline was used as a...

This paper describes a method for blind estimation of sharpness and resolving power from a single image. These measures can be used to characterize images in the context of the performance of image analysis procedures. The method assumes the point spread function (PSF) can be approximated by an anisotropic Gaussian. The width of the PSF is determined by the ratio of the standard deviations of t...

The aim of this paper is to extend the split-step idea for the solution of fractional partial differential equations. We consider the multidimensional nonlinear Schr"{o}dinger equation with the Riesz space fractional derivative and propose an efficient numerical algorithm to obtain it's approximate solutions. To this end, we first discretize the Riesz fractional derivative then apply the Crank-...