In the present paper are described experiments with synthetic polysaccharides prepared with muscle, heart, and liver phosphorylase. As judged by solubility properties and iodine colorations, the muscle enzyme synthesizes a polysaccharide in vitro which resembles plant starches, while the heart and liver enzymes synthesize a polysaccharide which resembles glycogen (1). It will be shown below tha...

in this research zinc oxide (zno) nano-crystalline powders were prepared by sol-gel method using zinc acetate. the zno nanoparticles were characterized by x-ray diffraction (xrd), scanning electron microscopy (sem), ultraviolet-visible (uv-vis), fourier transform infra-red (ft-ir) and energy dispersive x-ray (edx) spectroscopy. the structure of nanoparticles was studied using xrd pattern. the c...

among different spd techniques, equal channel angular pressing has attracted the most attentions,because of applying large strain to solid bulk materials. in this research, ecap process up to 6passes was carried out on a pure copper and a 6012 al-mg-si alloy with bc route in ecap dieswith φ=120 and ψ=20 and diameter of 20and 10 millimeter respectively. moreover, x-raydiffraction (xrd) system wa...

In the present study, new multi-components spinel ferrite Zinc doped metallic ferrites are investigated. The synthesized compounds consisting of Zinc copper ferrite nanostructures were developed using the Co-precipitation technique. Powder X-ray diffraction pattern (XRD) confirms the formation of the spinel phase for all the samples. The lattice constant was studied through powder X-ray diffrac...

In X-ray section topography of Si 220 diffraction in a multiple Bragg-Laue mode, a moiré pattern is observed when the incident beam is divided into two parts by inserting a platinum wire in the middle of the beam. The moiré pattern can be explained by the summation of two interference fringes corresponding to the two incident beams. The coherency of the X-rays from the bending-magnet beamline i...

Our present work presents a direct association of the observed loss of shear strength in boron carbide under plane shock wave compression to amorphization in boron carbide under triaxial stress compression. This evidence is obtained from in-situ measurement of Raman, and infrared vibrational spectra of boron carbide confined in a Diamond Anvil Cell (DAC) under hydrostatic and non-hydrostatic pr...

The thioborate phase Ba7(BS3)4S was synthesized from solid state reaction and its crystal structure determined by single crystal X-ray diffraction analysis. It crystallizes in the monoclinic space group C2/c (No. 15) with a = 10.1750(15) A, b = 23.970(4) A, c = 10.1692(15) A, beta = 90.095(2) degrees, and Z = 4. The structure consists of isolated trigonal planar (BS3)3- anions, and isolated S2-...

in this work firstly mgfe2o4 nanoparticles were synthesized via a microwave-assisted method. the product was calcinated at 900 ºc for 2h. at the second step zinc oxide shell was synthesized on the ferrite under ultrasonic waves. properties of the product were examined by x-ray diffraction pattern (xrd), scanning electron microscope (sem) and fourier transform infrared (ft-ir) spectroscopy. vibr...

Knowledge of the sequence of different conformational states of a protein molecule is key to better understanding its biological function. A diffraction pattern from a single conformational state can be captured with an ultrafast X-ray Free-Electron Laser (XFEL) before the target is completely annihilated by the radiation. In this paper, we report the first experimental demonstration of conform...

A pattern-fitting procedure for quantitative analysis of crystalline pharmaceuticals in solid dosage forms using X-ray powder diffraction data is described. This method is based on a procedure for pattern-fitting in crystal structure refinement, and observed X-ray scattering intensities were fitted to analytical expressions including some fitting parameters, i.e. scale factor, peak positions, p...