Heterogeneous catalysis performed in the liquid phase is an important type of catalytic process which is rarely studied in situ. Using microfocus X-ray fluorescence and X-ray diffraction computed tomography (μ-XRF-CT, μ-XRD-CT) in combination with X-ray absorption near-edge spectroscopy (XANES), we have determined the active state of a Mo-promoted Pt/C catalyst (NanoSelect) for the liquid-phase...

Hydrothermal and commercial barium titanate powders were examined for undesirable impurity phases. Compositional differences in the powder were evaluated using x-ray diffraction ( XRD ), x-ray fluorescence ( XRF ), and x-ray photoelectron spectroscopy (XPS). A brium-rich impurity phase, virtually undetectable by XRD, was detected via XPS. Barium impurity phase peaks were detected at binding ene...

Single crystalline zinc oxide (ZnO) nanowires have been grown on Si (100) substrates by a vapor-liquid-solid (VLS) process at temperatures in the range 850-950 °C in an inert atmosphere. The VLS-grown ZnO nanowires have been characterized in detail using X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), X-ray photoelectron spectroscopy (XPS), transmission electron mi...

Tellurium nanostructures have been prepared by physical vapor deposition method in a tube furnace. The experiments were carried out under argon gas flow at a pressure of 1 mbar. Tellurium powder was evaporated by heating at 350°C and 430°C and was condensed on substrates at 110–250°C, in the downstream of argon gas flow. The products were characterized by field emission scanning electron micros...

Tellurium nanostructures have been prepared by physical vapor deposition method in a tube furnace. The experiments were carried out under argon gas flow at a pressure of 1 mbar. Tellurium powder was evaporated by heating at 350°C and 430°C and was condensed on substrates at 110–250°C, in the downstream of argon gas flow. The products were characterized by field emission scanning electron micros...

Magnesium oxide nanoparticles were synthesized using Arabic gum as a biotemplate andmagnesium nitrate as the magnesium source by the sol-gel method. This method has manyadvantages such as nontoxic, economic viability, ease to scale up, less time consuming andenvironmental friendly approach for the synthesis of MgO nanoparticles without using anyorganic chemicals. Nanoparticles were characterize...

in this study, the tio2 nanorods were synthesized from p25 tio2 nanoparticles by hydrothermal method in 10 m naoh solution. the effects of annealing temperatures on produced nanorods were investigated  by scanning  electron microscopy (sem) x-ray diffraction (xrd) and photoluminescence (pl) spectroscopy. diameter growth and  changes  of  surface  oxygen  defects of  synthesized nanorods are stu...

zns  nanoparticles  were  synthesized  via  a  simple  surfactant  free microwave  route.  in  this  synthesis, thioacetamide  was  used  as sulfur  source.  the effects  of different  parameters  such  as  type of zinc precursor,  time  and  power  of  irradiation  on  the  morphology and  particle  size  of  the  products  have been  investigated.  the nanostructures  were  characterized  by ...

SnCl4/nano-sawdust was prepared as a carbohydrate-based catalyst containing of tin bearing cellulose units. The catalyst was characterized by X-ray diffraction (XRD), fourier transform infrared spectroscopy (FT-IR), field emission scanning electron microscopy (FESEM) and energy dispersive X-ray spectroscopy (EDS). The catalyst was applied successfully as a readily available, inexpensive, biodeg...

Transparent conducting oxide (TCO) materials are implemented into a wide variety of commercial devices because they possess a unique combination of high optical transparency and high electrical conductivity. Created during the processing of the TCOs, defects within the atomic-scale structure are responsible for their desirable optical and electrical properties. Therefore, studying the defect st...