the synthesis and single-crystal x-ray structure determination of the title compound (dinitrato) (1,4,8,11 -tetra-azaandecane) lead(ii) is described. crystals are monoclinic, p2 /ca= 10.271 (2)?,b= 13.524(4) ?,c= 11.298(6) ?,?=94.68(3),2=4,r,rw, 0.036 and 0.041, respectively. the lead atom is eight-coordinate [pb-n, 2.44 (2) - 2.55 (1)], [pb-0,2.87 (1) - 3.06 (2)].

elstic properties of nickel single crystal has been studied in magnetie fields ranging from 0 to 12 kgauss. comparison of the observed data shows that there might be an effect of changes in the rate of elongation due to the strangth of magnetic field in proportional region.

As a result of switching the growth from hexagonal disks to nanorods/nanobelts, single-crystalline ‘nanocastles’ of ZnO have been synthesized. This new structure was constructed by two basic parts: a sheet-like hexagonal crystal base and vertical nanorods/nanobelts surrounding the base as the ‘walls’ of the castle. Moreover, for the first time, ZnO nanorods with a triangular and diamond cross-s...

Several experiments have been performed to probe the enantiospecific properties of chiral single crystal surfaces. The surfaces chosen have been the (643) planes of Ag and Cu, both face centered cubic structures. The chirality of these surfaces arises from the handedness of their kinked step structures. These structures are such that the (643) and the (643) surfaces are related by mirror symmet...

Understanding a simple crystal oscillator transmitter circuit The transistor in common emitter configuration contributes -180 deg phase shift between base. Write short notes on (i) RC Oscillator (ii) Wien bridge Oscillator (iii) Crystal It consists of a conventional single transistor amplifier and a RC phase shift network. The wien-bridge oscillator is the standard oscillator circuit for all fr...

SiC single crystal is usually grown by sublimation (modified Lely method). There is a lotof remaining issues that should be solved. One is the technical problems of SiC single crystal growth process. And the other is the theoretical problem based on SiC physical properties. As the example of technical issues, in this paper, the example of design optimization for SiC sublimation growth is descri...

The magnetization, specific heat and electrical resistivity of PrRhIn5 compound were studied. High quality crystals of PrRhIn5 and LaRhIn5, which adopt the tetragonal HoCoGa5-type (P4/mmm) structure, were prepared by solution growth. In the range 150 320 K the susceptibility χ follows the Curie-Weiss law. For PrRhIn5 the effective moment μeff and paramagnetic Curie temperature θp are μeff = 3. ...

single-walled carbon nanotubes (swcnt) and multi-walled carbon nanotubes(mwcnt) were melt-blended with polyvinylidene fluoride (pvdf).ft-ir technique revealed that swcnt has insignificant effect on the crystalline structure of pvdf and at 3wt% modification only 14% beta crystal isformed. this observation was accounted for by the chair structure of swcnt. in mwcnt nancomposites it was found that...

Crystals of the title dysprosium tin sulfide oxide, Dy(8)SnS(13)S(1-x)O(x) [x = 0.39 (4)], were obtained unintentionally from the Dy-Sn-S system. A statistical mixture of sulfur and oxygen was assumed for one position in the structure. S and O atoms surround each of the eight symmetrically non-equivalent dysprosium atoms. The Sn atoms are located in tetra-hedral surroundings of sulfur atoms. Tr...