the aim of this study was to investigate the sol gel synthesis of ha/fa nanoparticles and the possible formation of tcp phase or unstoichiometric calcium deficient hydroxyapatite (cdha) from the precursors with a ca/p ratio of 1.62. in order to prepare the sol, the solutions of triethyl phosphite, ammonium fluoride and calcium nitrate in ethanol were used respectively as p, f and ca precursors....

background: radioactive yttrium glass microspheres are used for liver cancer treatment. these yttrium aluminum silicate microspheres are synthesized from yttrium, aluminum and silicone oxides by melting. there are two known processes used to transform irregular shaped glass particles into microspheres, these ‘spheroidization by flame’ and ‘spheroidization by gravitational fall in a tubular furn...

the photocatalytic coatings were prepared via incorporating the modified titania nanoparticles into epoxy-based inorganic-organic hybrid coatings. titania nanoparticles were first synthesized from tetra-n-butyl titanate using sol-gel methods by two different calcination treatments, i.e., in mild condition (80°c) and 500°c. the formed anatase nanoparticles were further modified as titania-silica...

cumn2o4 nanoparticles, a semiconducting materials with tunable functionalities in solid oxide fuel cell, was successfully synthesized via a sol-gel method using its respective metal cations sources i.e. cu2+ and mn2+ in an appropriate complexing agent.the vibrational frequencies below 1000 cm-1 of the obtained materials confirmed the formation of metal-oxygen (m-o:cu-o, mn-o) bond in the sample...

AbstractVarious nanoparticles have been investigated as novel drug delivery systems, including solid lipid nanoparticles (SLNs). Due to their rapid clearance from systemic circulation, nanoparticles do not provide sustained action in most cases. Different strategies have been employed to overcome this problem. In this direction, the present study introduces erodible in-situ forming gel systems ...

Electrically driven liquid jets are combined with sol-gel methods to design vesicles and fibers made from inorganic oxides and hybrid materials with diameters in the micrometer and submicrometer range. The proposed materials synthesis method benefits greatly from the maturity of sol-gel chemistry and the generalities of a structure-directing phenomenon that is physical in nature.

nano zno/ montmorillonite composite were prepared by sol gel method under ultrasonic irradiation from directly mixing montmorillonite nano clay into zinc gel. the zn(ch3coo)2.2h2o and montmorillonite nano clay was used as precursor. the zinc acetate was dissolved in di water and, nh3 (aq) solution was dropped into the zinc solution until ph 9 consequently the zinc gel was produced. the montmori...

limn2o4 spinel cathode materials have been successfully synthesized by solid-state reaction. surface of these particles were modified by nanostructured lifepo4 via sol gel dip coating method. synthesized products were characterized by thermally analyzed by thermogravimetric and differential thermal analysis(tg/dta), x-ray diffraction (xrd), scanning electron microscopy (sem), and energy dispers...

in this paper, zno thin film is deposited on slide glass substrate using the sol-gel process. presenting well-defined orientation of zno thin films nanostructure were obtained by dip coating of zinc acetate dihydrate, monoethanolamine (mea), de-ionized water and isopropanol alcohol. the annealed zno thin films were transparent ca 85-90% in visible range with an absorption edges at about 375 nm....

high purity fluorapatite (fa) with rod-like and spherical-like morphology was synthesized via sol-gel method. chemical characterization of fa powders was done by xrd and ftir analyses. crystallite samples were calculated using scherer method. morphology of fa powders was investigated with tem and sem images. the results revealed that increasing the time of hydrolysis of phosphate sols significa...