نتایج جستجو برای: solvothermal process

تعداد نتایج: 1313854  

2013
N. Saraswathi N. Neelakanda Pillai C. K. Mahadevan

Nano-structured Zinc oxide is of high potential importance and has wide range of applications. We have made an attempt to investigate the effect of adding Mn 2+ and S 2separately as dopants on the structural, optical, and magnetic properties of nano-structured ZnO. A total of five samples pure and Mn 2+ and S 2added each with two different concentrations viz. 2.5 and 5.0 weight percentages were...

Journal: :Chemical communications 2006
Hui Qiao Falong Jia Zhihui Ai Zhaosheng Li Lizhi Zhang

Spring-like superstructures consisting of layered tin(IV) hydrogen phosphate nanodisks can be obtained via a one-pot solvothermal reaction of tin tetrachloride and phosphoric acid in ethanol. These superstructures are active anode materials for the lithium-ion battery.

Journal: :Chemical communications 2015
Wei Zhou Jinxian Wang Feifei Zhang Shumin Liu Jianwei Wang Dongming Yin Limin Wang

A SnO2-N-doped graphene (SnO2-NG) composite is synthesized by a rapid, facile, one-step microwave-assisted solvothermal method. The composite exhibits excellent lithium storage capability and high durability, and is a promising anode material for lithium ion batteries.

Journal: :The Analyst 2014
Xiaoyue Shan Lujing Chai Juanjuan Ma Zhaosheng Qian Jianrong Chen Hui Feng

Fluorescent B-doped carbon quantum dots (BCQDs) were prepared by a facile one-pot solvothermal route. The BCQDs can be used as a novel fluorescence sensing system for hydrogen peroxide and glucose detection.

2016
Ruxue Li Xiaohua Wang Xinwei Wang Haoran Zhang Jingxin Pan Jilong Tang Dan Fang Xiaohui Ma Yongfeng Li Bin Yao Jie Fan Zhipeng Wei

Uniform antimony (Sb) nanotubes were successfully synthesized via a facile solvothermal method without the need for any surfactants or templates. The Sb nanotubes are confirmed to be pure rhombohedral phase and have better crystallinity. These nanotubes show middle-hollow and open-ended structures, as well as multi-walled structures with the wall thickness of about 10 nm. Also, they have an ave...

2013
Zhengde Tan Fengjiao Tan Li Zhao Junyong Li

In our work, ciprofloxacin was extracted from the raw material ciprofloxacin hydrochloride and coordinated with the metal ions of copper, manganese and zirconium. The procedures include the comparison of the autoclave method with the solvothermal method, synthesizing the corresponding complexes and conducting antibacterial test on nearly 20 kinds of bacteria. It is shown that under the conditio...

Journal: :Nanoscale 2016
Xiaoyan Zhang Saifeng Zhang Bohua Chen Hao Wang Kan Wu Yang Chen Jintai Fan Shen Qi Xiaoli Cui Long Zhang Jun Wang

Hierarchical MoS2 thin films nanostructured with orthogonally oriented vertically and horizontally aligned layers were designed and excellent passive Q-switching behavior in a fiber laser was demonstrated. A special solvothermal system containing a small amount of water was applied to synthesize such hierarchical MoS2 nanofilms, in which the reaction rate is carefully controlled by the diffusio...

Journal: :Dalton transactions 2009
Ian S Tidmarsh Luke J Batchelor Emma Scales Rebecca H Laye Lorenzo Sorace Andrea Caneschi Jürgen Schnack Eric J L McInnes

The crystal structure of the monomeric vanadium(III) species mer-[V(bipy)Cl(3)(MeCN)] (1; bipy = 2,2'-bipyridine) is reported. The solvothermal reaction of [V(bipy)Cl(3)(MeCN)]with Na(O(2)CPh) yields the T-shaped cluster [V(3)(O)Cl(3)(O(2)CPh)(2)(bipy)(2)(OEt)(2)], magnetic studies of which show strong intramolecular antiferromagnetic coupling giving a well isolated S = 1 ground state. Solvothe...

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