SINGLE CRYSTALS OF THE NEW TITLE COMPOUND [SYSTEMATIC NAME: 1,4,7,10-tetra-zoniadecane hexa-chloridorhodate(III) chloride], [H(3)N(CH(2))(2)NH(2)(CH(2))(2)NH(2)(CH(2))(2)NH(3)][RhCl(6)]Cl, were obtained from the corresponding amine and rhodium trichloride in hydro-chloric acid solution by slow crystallization under diffusion-controlled conditions at room temperature. Its solid-state structure i...