Influence of organic biphasic pretreatment on levoglucosan (LG) yield from biomass pyrolysis was investigated with dilute sulfuric acid and sodium hydroxide as comparison, simultaneously, the mechanism explored in depth. It found that monophasic (water) conditions, pretreatment, LG all increase largely (from untreated 28% to treated 60–85%) due removal hemicellulose or lignin. Phenoxyethanol in...