This paper describes the development of a procedure for Pb(II) ions removal from various water samples after magnetic solid phase extraction (MNPs) by magnetite nanoparticles (Fe3O4 NPs) modified with sodium dodecyl sulfate (SDS) and pyrrolidine-1-dithiocarboxylic acid ammonium (PDTCAA). The synthesis of Fe3O4 NPs was certified by characterization techniques including field emission scanning el...

The present article reports on the application of modified organo nanoclay as a green, easily prepared and stable solid sorbent for the preconcentration of trace cobalt ion in aqueous solution. The organo nanoclay was modified by adsorption of 5-(4-dimethyl amino-benzylidene) rhodanin reagent onto it. The sorption of Co2+ ions was quantitative in the pH range of 7.0 to 8.5, whereas quantitative...

In this work, we developed a method based on ultrasound-assisted emulsification microextraction (USAEME) for the determination of zinc and copper by flame atomic absorption spectrometry (FAAS). The method is based on the use of the organic solvent carbon tetrachloride (CCl4) as an extraction solvent. In order to obtain a high enrichment factor, the effect of different parameters affecting the c...

This study focus on the preparation of two supports including activated carbon derived from medlar and Palladium nanoparticles loaded on activated carbon (Pd-NP-AC). Subsequently, both adsorbent modified with a novel Schiff base chelating agent and their potential applicability for determination of trace amounts of metal ions from aqueous solution has been investigated. The method is based on c...

in the present study, the concentrations of three heavy metals including lead (pb), zinc (zn) and arsenic (as) in 72 different honey samples collected from north-western regions of iran were investigated using atomic absorption spectroscopy method. all metals were detected in 88.88% of the honey samples. the range of metals contamination in honey samples was 0.01 to 11.09 ppm. zn was the most a...

A simple and rapid microextraction procedure based on dispersive liquid-liquid microextraction (DLLME) was developed for determination and speciation of trace amounts of chromium (Cr) by flame atomic absorption spectrometry (FAAS). In the proposed approach, chloroform and methanol were used as extraction and dispersive solvents. A new Schiff's base ligand, bis(2-methoxy benzaldehyde) ethylene d...

A simple, highly sensitive, accurate and selective method for determination of trace amounts of Pb(II) in water samples is presented. A novel Graphene oxide with covalently linked porphyrin solid-phase extraction adsorbent was synthesized by covalently linked porphyrin onto the surfaces of graphite oxides. The stability of a chemically (GO-H2P) especially in concentrated hydrochloric acid was s...

A simple, highly sensitive, accurate and selective method for determination of trace amounts of Co(II) in water samples is presented. Isocyanate treated graphite oxides (iGOs) solid phase extraction adsorbent was synthesized by covalently isocyanate onto the surfaces of graphite oxides. The stability of a chemically (iGOs) especially in concentrated hydrochloric acid which was then used as a re...

This paper describes the development of a procedure for Pb(II) ions removal from various water samples after magnetic solid phase extraction (MNPs) by magnetite nanoparticles (Fe3O4 NPs) modified with sodium dodecyl sulfate (SDS) and pyrrolidine-1-dithiocarboxylic acid ammonium (PDTCAA). The synthesis of Fe3O4 NPs was certified by characterization techniques including field emission scanning el...

A simple, highly sensitive, accurate and selective method for determination of trace amounts of Co(II) in water samples is presented. Isocyanate treated graphite oxides (iGOs) solid phase extraction adsorbent was synthesized by covalently isocyanate onto the surfaces of graphite oxides. The stability of a chemically (iGOs) especially in concentrated hydrochloric acid which was then used as a re...