Zusammenfassung In dieser Arbeit wird ein Elektroneneinfangdetektor basierend auf weicher Röntgenionisation mit vergleichbarer Performance bezüglich radioaktiver Elektroneneinfangdetektoren geringsten Nachweisgrenzen im pptv-Bereich und einer Linearität über drei Größenordnungen vorgestellt. werden freie Elektronen erzeugt deren Menge die Entladung an Faraday-Detektorplatte ermittelt. Eintreten...

A gas chromatographic method was developed for the simultaneous determination of 12 pyrethroids (tefluthrin, bifenthrin, fenpropathrin, cyhalothrin, permethrin, cyfluthrin, cypermethrin, alpha-cypermethrin, flucythrinate, fenvalerate, fluvalinate, and deltamethrin) in tomato puree, peach nectar, orange juice, and canned peas. A miniaturized extraction-partition procedure requiring small amounts...

mass spectrometry analysis of lipopolysaccharide-derived 3-hydroxy fatty acids. Gram-negative cell walls were also measured by using two-dimensional gas chromatography/electron-capture analysis of diaminopimelic acid originating from the peptidoglycan. The correlation between the results of the Limulus assay and those of gas chromatography-mass spectrometry for determination of the lipopolysacc...

BACKGROUND Asian traditional herbal preparations are frequently considered for the contamination with undeclared toxic or hazardous substances. The aim of this study was to determine the toxic heavy metals, pesticides and sulfur dioxide in decoctions that is a common form of final utilization in Korea. METHODS A total of 155 decoctions composed of multi-ingredient traditional herbs were rando...

found in the response of the electron-capture detector for fatty acids of niicrosomal lipids from CC1,-treated rats (the latter peak is clearly a group of unresolved peaks). Since serum very-low-density lipoproteins derive directly from the hepatic cell and since the phospholipid fraction of such lipoproteins is believed to derive from the phospholipids of the endoplasmic reticulum, we investig...