In drug discovery research, residual solvent measurement is an integral part of purity analysis for synthesis of a drug candidate before it is used for toxicity testing. This is usually carried out using gas chromatography (GC) with direct injection sample introduction. This method requires testing compounds to be soluble at high concentrations (>50 mg/mL, usually in DMSO) to achieve acceptable...

In this study, the comparison and monitoring of the initial greenhouse gas (GHG) emissions using a flux chamber and gas analyzer from three different liquid manure application methods at a swine farm in Kentucky were carried out. Swine slurry was applied to farmland by row injection, surface spray, and Aerway injection. Ammonia and GHG concentrations were monitored immediately after application...

the study of interactions of jet into cross flow at different longitudinal and transverse angles ofjet was studied. the following components were designed and constructed: a low velocity windtunnel to produce the uniform flow, a flat plate with a traverse injection system to simulate the jetinjection, and a spatial rake to measure the total pressure. the tests were carried out atlongitudinal (α...

Microscopic oil displacement of water flooding and sweep efficiency of continuous gas injection could be improved by water alternating gas (WAG) injection. The WAG injection process aims to squeeze more oil out of the reservoirs; in this method, water and gas are alternatively injected into the reservoir. Also, availability of hydrocarbon or CO2 gases in the field makes it attractive for gas-ba...

Afferent signaling via the vagus nerve transmits important general visceral information to the central nervous system from many diverse receptors located in the organs of the abdomen and thorax. The vagus nerve communicates information from stimuli such as heart rate, blood pressure, bronchopulmonary irritation, and gastrointestinal distension to the nucleus of solitary tract of the medulla. Th...

A fluorescência natural da ibuprofeína foi melhorada quando foi formado um complexo convidado-hospedeiro com a beta-ciclodextrina (beta-CD). A partir disso, foi desenvolvido um método por injeção em fluxo para a determinação de ibuprofeína em diferentes preparações farmacêuticas, com detecção fluorescente (λ em 287 nm, λ ex 233 nm). A curva de calibração foi linear no intervalo entre 6,00 a 60,...

An injection unit is considered as a speed control system utilizing a reaction-force sensor. Our purpose is to design a fault detector that detects and isolates actuator and sensor faults given that the system is disturbed by a reaction force. First described is the fault detector’s general structure. In this system, a disturbance observer that estimates the reaction force is designed for the s...