The synthesis of Nb doped BaTiO3 has been investigated under Microwave-Hydrothermal (MH) conditions in the temperature of 150°C for only 2 h using C16H36O4Ti, BaH2O2.8H2O and NbCl5 as Ba, Ti and  Nb sources, respectively.  Typical experiments performed on MH processing have not yet reported for Nb doped BaTi...

Tungsten oxide (WO3) and tungsten oxide hydrate (WO3.H2O) nanoparticles were synthesized via microwave-assisted solution combustion in comparison with the acidic precipitation method. Oxalic acid was used as a surfactant and forming agent in the acidic precipitation method. In addition to oxalic acid, glycine and citric acid were also used as fuels in the microw...

Nan-sized inorganic particles having characteristic morphology and narrow size-distribution have attracted attention due to their potential applications as functional materials, i.e., catalysts, magnetic materials, conducting inks, and ferrofluids. Various preparation and stabilization methods of nano-sized metal particles, metal oxide particles, and metal sulfide particles have been reported. ...

Effects of ionic liquid structures on the aluminophosphate molecular sieve products in ionothermal synthesis process were investigated. The results showed that the possible structure-directing effect of ionic liquid might exist during ionothermal synthesis. Microwave heating was introduced into the ionothermal synthesis, which led to a fast and safe process for preparation of molecular sieves. ...

Microwave energy (MWe) is, nowadays, widely used as a clean synthesis tool to improve several chemical reactions, such as drug molecule synthesis, carbohydrate conversion and biomass pyrolysis. On the other hand, its exploitation in enzymatic reactions has only been fleetingly investigated and, hence, further study of MWe is required to reach a precise understanding of its potential in this fie...

Ultra-fast and large-quantity (grams) synthesis of one-dimensional ZnO nanowires has been carried out by a novel microwave-assisted method. High purity Zinc (Zn) metal was used as source material and placed on microwave absorber. The evaporation/oxidation process occurs under exposure to microwave in less than 100 s. Field effect scanning electron microscopy analysis reveals the formation of hi...

Objective(s): In this work, pomegranate juice was used as a capping agent for self- assembly to form particles-like Au nanostructures in the presence of AuHCl4.3H2O as aurate source. Besides, to investigate the concentration effect of pomegranate juice as the green capping agent on the morphology and particle size of final products several experiments were...

This review describes the recent advances in the microwave-assisted synthesis of 7-membered and larger heterocyclic compounds. Several types of reaction for the cyclization step are discussed: Ring Closing Metathesis (RCM), Heck and Sonogashira reactions, Suzuki-Miyaura cross-coupling, dipolar cycloadditions, multi-component reactions (Ugi, Passerini), etc. Green syntheses and solvent-free proc...

BACKGROUND Curcumin and vanillin are the two useful compounds in food and medicine. Bismuth nitrate pentahydrate is an economical and ecofriendly reagent. METHOD Bismuth nitrate pentahydrate impregnated montmorillonite KSF clay and curcumin were subjected to microwave irradiation. RESULTS Microwave-induced bismuth nitrate-promoted synthesis of vanillin from curcumin has been accomplished in...

Combination of the surfactant-free nonaqueous sol–gel approach with the microwave technique makes it possible to synthesize Fe3O4, CoFe2O4, MnFe2O4, and NiFe2O4 nanoparticles of about 5–6 nm and with high crystallinity and good morphological uniformity. The synthesis involves the reaction of metal acetates or acetylacetonates as precursors with benzyl alcohol at 170 C under microwave irradiatio...