several samples of mesoporous silica were prepared via sol-gel chemistry in the presence of ctab as template with variation of stirring intensity and aging time, ratios of ctab/sio2 and nh4oh/h2o in synthesis mixture. effects of aging temperature, hydrothermal treatment and ter-butanol addition to the synthesis mixture on the textural properties of obtained samples were also studied. results of...

The processing of ceramic scaffolds using the ice-templating, or freeze casting, technique provides a relatively simple means to mimic the hierarchical design of natural materials such as nacre. In the present study, we investigated the architecture of silicon carbide (SiC) scaffolds produced by this technique over a range of cooling rates and suspension characteristics to demonstrate its versa...

In this paper, we focused on the effects of initial solution’s pH on the composition, structure and morphology of hydrothermally synthesized titanium oxide nanoparticles. TiCl4 and NaOH were used as titanium source and precipitant, respectively. Phase and structure determination of samples were obtained by X-ray diffraction (XRD) analysis. Scanning electron microscopy (SEM) images were used for...

The research investigates synthesized Nano-structured PbO2 using ball milling. The structure and morphology of the samples were determined in the process of milling by means of XRD and SEM. The size of particles was estimated through DLS analysis. The TEM image of the synthesized powder verifies the achievement of Nano dimensions. Design and analyses of the results using Taguchi methodology rev...

Silver nanostructures as an effective antibacterial materials were synthesized via three various hydrothermal, sono-chemical and microwave methods using water as a green solvent. Then Chitosan-Ag polymer based nanocomposites were made by a fast chemical procedure. The influence of power, temperature and time on the morphology and particle size of the products was investigated. Scanning electron...

The size and morphology of particulate polyvinyl alcohol (PVA) sponge prepared by a blender technique for embolotherapy were analyzed by light and scanning electron microscopy. Techniques for preparation and sizing of PVA sponge particles are described. Two types of particulate material, differing in both size and morphology, were found. Large particles (greater than 50 micron) had irregular sh...

Inflectional affixes are sensitive to morphological properties of the elements they attach to. Therefore Bierwisch (1987) suggested that the inflectional material is combined with both the verbal stem of simplex verbs and the verbal stem of particle verbs. He argued that this leads to the bracketing paradox in the case of particle verbs since the semantic contribution of the inflectional inform...

A facile co-precipitation method for the synthesis of well-dispersed NdFeO3 nanocrystals is developed in the presence of octanoic acid as surfactant. Co-precipitation can produce fine, high-purity, stoichiometric particles of single and multicomponent metal oxides. The product is characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), scanning electron microsc...