in this research, a rapid, reliable and selective dispersive liquid-liquid microextraction (dllme) followed by direct injection of microdroplet to graphite furnace atomic absorption spectrometry (gf-aas) method for the determination of ultra-trace amounts of ag(i) was developed. effect of the important experimental parameters on the extraction efficiency of ag(i) was investigated using response...

This report investigates the use of solvent-solvent extraction for the secondary concentration of lead and thorium. The extraction reagents investigated in this report are: For the lead extraction: diethlyammonium diethyldithiocarbamate (DDDC) For the thorium extraction: trioctylphosphinc oxide (TOPO) and di-(2-ethylhexyl)phosphoric add (HDEHP). For all of the extractions 2-octanone was used as...

Background: A syringe to syringe dispersive liquid phase micro-extraction-floating organic drop was applied and used for the simultaneous extraction and pre-concentration of trace amounts of amphetamine (AMP) and methamphetamine (MAMP) in urine samples. The extracted analytes were determined by high performance liquid chromatography along with diode array detection. Materials & Methods: In thi...

A simple, rapid and efficient method has been developed for the extraction, preconcentration and determination of cobalt (II) and nickel (II) ions in water samples by air-assisted liquid-liquid microextraction (AALLME) coupled with graphite furnace atomic absorption spectrometry (GFAAS). In the proposed method, much less volume of an organic solvent was used as the extraction solvent in the abs...

cinnamon is the bark the cinnamomi cassia that exhibits many medical properties such as anti-cancer effect and anti-diabetic effect. moreover, because of its antioxidant activity; it can be used in food industries. many studies have already reported biological and chemical properties of the cinnamon extracted essential oil such as their antimicrobial, antifungal, antimosquito, free radical scav...

urinary 1-hydroxypyrene is frequently used as a major metabolite and biological indicator of the overall exposure to polycyclic aromatic hydrocarbons. in this study, solid phase extraction was appropriately conditioned with regard to sample ph, sample concentration, loading flow rate, elution solvent, washing solvent, sample volume and sorbent mass. octadecyl silica cartridge (c18) was used as ...

A method based on the ultrasound-assisted solidification of floating drop microextraction technique was developed for the spectrophotometric and spectrofluorimetric determination of curcumin in turmeric powder. In this work a small volume of an organic solvent was floated on the surface of an aqueous solution. After sonication the organic solvent is solidified and separated. The effect of extra...

abstract: chemical composition of lavandula angustifolia was studied by solvent free microwave extraction (sfme) and hydrodistillation (hd) methods. 1, 8-cineole (42.7% and 37.9%), camphor (26.1% and 21.3%) and borneol (31.2% and 21.6%) were the major compounds that obtained by sfme and hydrodistillation, respectively. the antibacterial activity of extracted oils was investigated against gram-p...

The objective of this study was to compare the oil extraction yield and essential oil composition of Indian and Iranian Nigella sativa L. extracted by using Supercritical Fluid Extraction (SFE) and solvent extraction methods. In this study, a gas chromatography equipped with a mass spectrophotometer detector was employed for qualitative analysis of the essential oil composition of Indian and Ir...