BACKGROUND AND METHODS Several standard powdered black pigments were characterized by means of thermogravimetry TG-DTG and allied techniques. These pigments were used to make standard plaster frescoes at this purpose prepared. The latter ones were subjected to Raman and reflectance analysis. The results obtained, together with TG data, were chemometrically processed and used to identify an anal...

Thermal decomposition kinetics of calcium carbonate was studied by non-isothermal thermogravimetric analysis at different heating rates. The reaction mechanism was found to follow a two-dimensional phase boundary-controlled model by modelfree and model-fitting methods. Two non-Arrhenius equations (Harcourt–Esson equation and Berthelot–Hood equation) were used to interpret the decomposition kine...

Thermal decomposition and kinetics behaviour of the de-oiled seed cake of African star apple (Chrosophyllum albidum) has been investigated using thermogravimetry under the nitrogen atmosphere from ambient temperature to 900 °C. The thermogravimetric data for the cake decomposition at six different heating rates (5, 10, 15, 20, 30 and 40 °C/min) were used to evaluate the kinetic decomposition of...

The compound lead oxide sulfate PbSO4.PbO was prepared in our laboratory. The Thermal behavior of PbSO4 was studied using techniques of Thermogravimetry under air atmosphere from 25 to 1200 ̊C. The identity of both compounds was confirmed by XRD technique. Results obtained using both techniques support same decomposition stages for this compound. The electron microscopic investigations are made ...

So far, hydrogen compatibility of polymer materials was investigated, focusing on gaining insight in general degradation mechanisms. However, this is not yet sufficient for purposes safety and performance requirements, example, the automotive industry especially, corresponding advanced material development, which needs meaningful comprehensive data prospective long time intervals. Therefore, he...

The paper evidences changes of thermal properties of poly(methyl methacrylate) as well as methyl methacrylate copolymers with glycidyl methacrylate (GMA) polymers synthesized classic and comparatively in a magnetic field. Samples of poly(methyl methacrylate) and methyl methacrylate copolymers with different amounts of GMA synthesized by radical emulsion polymerization with or without the presen...

In this study Klason lignins from Eucalyptus grandis (LEUG) and Pinus taeda (LPIT) were characterized using Fourier transform infrared (FTIR) spectroscopy and thermogravimetry (TGA). The degradation kinetic parameters were determined by TGA using the Kissinger method. Thermogravimetric results showed that LPIT had higher thermal stability and also higher activation energy than LEUG. FTIR result...