in this work firstly fe3o4 nanoparticles were synthesized via a sono-chemical method. at the second step magnesium hydroxide shell was synthesized on the magnetite-core under ultrasonic waves. for preparation fe3o4-mgo the product was calcinated at 400 ºc for 2h. properties of the product were examined by x-ray diffraction pattern (xrd), scanning electron microscope (sem) and fourier transform ...

In this work, Fe3O4@SiO2 core-shell nanocomposites were successfully synthesised via a simple co-precipitation method. X-ray diffraction pattern of clearly shows the existence main phase Fe3O4, beside an amorphous structure SiO2. The with average particle size in range 10-20 nm is observed by SEM and TEM images. FTIR spectrum illustrates Fe-O Si-O-Si bonds sample, indicating formed nanocomposit...

In this research, a sol-modified composite electrodeposition technique that combines the sol-gel method with the conventional electrodeposition process was utilized to deposit Ni-TiO2 nanocomposite coatings. Cyclic voltammetry and chronoamperometry techniques were applied to study the influence of the TiO2 sol concentration on the deposits’ electrochemical behavior. The results clearly showed t...

In this study, nanometer sized of Ag/Fe3O4 nanocomposite (AFN) have been synthesized by using a simple and based on chemical reduction method. The size and shape of (AFN) controlled by using of condensation (Fe2O3 (2.975 mmol), NaBH4 (21.25 mmol), AgNO3 (2.532 mmol) and polyvinylpyrrolidone (PVP) (8.925 mmol K30 Mr=10.000) in 40 ºC. The synthesized AFN was characterized by XRD, scanning electro...

Nanocomposites of multi-walled carbon nanotubes and titanium dioxide (MWCNT/TiO2) were synthesized by the sol-gel method. Regarding hydrophobicity of carbon nanotubes (CNTs), benzyl alcohol was used as the linking agent between CNT powder and TiO2 gel which was prepared from the precursor of titanium tetraisopropoxide. The prepared samples were treated under thermal treatments. A part of the sa...

this study aims at exploring an effective route in the in situ graft polymerization of aniline from fe3o4 nanoparticles. to this goal, fe3o4 magnetic nanoparticles were prepared by coprecipitation method using ammonia solution as the precipitating agent, and were characterized by fourier transform infrared (ft-ir) spectroscopy, x-ray diffraction (xrd) and transmission electron microscopy (tem)....

Nanocomposite of Ag/TiO2 and nanocrystalline TiO2 were prepared by using TiCl4 as a precursor in a simple sol-gel process. The prepared photo-catalysts were characterized by X-ray diffraction (XRD), scanning electron micrographs (SEM), energy dispersive X-ray microanalysis (EDX), transmission electron microscopy (TEM) and diffuse reflectance spectroscopy (DRS). A complete and effective photocat...

Magnetic nanoparticles (MNPs) are very important systems with potential use in drug delivery systems, ferrofluids, and effluent treatment. In many situations, such as in biomedical applications, it is necessary to cover inorganic magnetic particles with an organic material, such as polymers. A superparamagnetic nanocomposite Fe3O4/poly(maleic anhydride-co-acrylic acid) P(MAH-co-AA) with a core/...

We report an environmentally friendly synthetic strategy to fabricate reduced graphene oxide (rGO)-based ternary nanocomposites, in which glutathione (GSH) acts both as a reducing agent for graphene oxide and sulfur donor for CdS synthesis under modified hydrothermal (MHT) conditions. The report becomes interesting as pH variation evolves two distinctly different semiconducting nanocrystals of ...