1. Abstract 2. Introduction 3. Experimental procedures 3.1. Reagents 3.2. Apparatus 3.3. Electrode preparation 4. Results and discussion 4.1. Preparation and characteristics of nano-SnO2 4.1.1. The preparation of nanoSnO2 4.1.2. The characteristics of nano-SnO2 4.2. Electrochemical behaviors of CFX at the nano-SnO2 modified electrode 4.2.1. Cyclic voltammograms of CFX at various modified electr...

In this article, the electrochemical behavior of triethanolimine is described with a carbon paste electrode. A differential pulse voltammetric method was also developed for the determination of triethanolamine as an application to electroanalysis at a carbon paste electrode. The resultant voltammograms have revealed the irreversible electrochemical process that can be utilized to quantify the s...

An electrochemical flow cell with a boron-doped diamond dual-plate microtrench electrode has been developed and demonstrated for hydroquinone flow injection electroanalysis in phosphate buffer pH 7. Using the electrochemical generator-collector feedback detector improves the sensitivity by one order of magnitude (when compared to a single working electrode detector). The diffusion process is sw...

We report on the aptadetection of chloramphenicol (CAP) using electrochemical impedance spectroscopy. The detection principle is based on the changes of the interfacial properties of the electrode after the interaction of the ssDNA aptamers with the target molecules. The electrode surface is partially blocked due to the formation of the aptamer-CAP complex, resulting in an increase of the inter...

Here, we report a nanopipette-based electrochemical approach to prepare metal nanoelectrodes with excellent control over electrode size, shape, and thickness of the insulation wall. Nanoelectrodes are prepared by electrochemical plating in a laser-pulled quartz nanopipette tip immersed in a liquid gallium/indium alloy electrode, which not only protects the ultrasmall quartz tip but also starts ...

The improvement of electrochemical detection of meloxicam is presented by modification of a glassy carbon electrode with anionic layer of cysteic acid providing electrostatic accumulation of the analyte onto the electrode surface. The modification formed by electrochemical oxidation of L-cysteine was performed by cycling potential in cysteine solution. The anodic peak current obtained at + 1.08...

Layered double hydroxides (LDHs), also known as hydrotalcite-like anionic clays, have been investigated widely as promising electrochemical active materials. Due to the inherently weak conductivity, the electrochemical properties of LDHs were improved typically by utilization of either functional molecules intercalated between LDH interlayer galleries, or proteins confined between exfoliated LD...

Co3V2O8 thin nanoplates are firstly described as a kind of electrode material for supercapacitors. More importantly, from electrochemical measurements, the obtained Co3V2O8 nanoplate electrode shows a good specific capacitance (0.5 A g(-1), 739 F g(-1)) and cycling stability (704 F g(-1) retained after 2000 cycles). This study essentially offers a new kind of metal vanadium oxides as electroche...

A three electrodes planar electrochemical sensor, based on CuO nanowires growth “in situ” on Cu working electrode, was fabricated by a simple micromachining technique and employed for the non-enzymatic determination of glucose. The microstructural and morphological characteristics of the modified electrode was investigated by XRD and SEM analysis. Cyclic voltammetry and chronoamperometric measu...

In the present paper, electrochemical methods were used to investigate the behavior of ascorbic acid at a carbon paste electrode modified with 2,2'-((1E)-(1,2 phenylenebis(azanylylidene)) bis(methanylylidene))bis(benzene-1,4-diol) (PBD) and oxidized multiwall carbon nanotubes. The modified carbon paste electrode showed high electrocatalytic activity toward ascorbic acid; the current was enhance...