In this project, a three-component functionalization of carboxylated shortend multi-walled carbon nanotubes (MWNT-COOH) by Histidine derivative via amidation method have been investigated. The functionalized MWNTs were characterized by Fourier Transform Infrared spectroscopy (FT-IR), Raman spectroscopy, elemental analysis and scanning electron microscopy (SEM). 

This perspective discusses the ways that advanced paramagnetic resonance techniques, namely electron-nuclear double resonance (ENDOR) and electron spin-echo envelope modulation (ESEEM) spectroscopies, can help us understand how metal ions function in biological systems.

Photosynthetic Electron Transport, Plastidic Cytochromes, Dual-Wavelength Spectroscopy, Cross-Over Experiments; Oxidation-Reduction Potentiometry Dual-wavelength spectroscopy allows the precise and fast measurement of small absorbance changes in highly absorbing and scattering samples (fS 10“ 3 absorbance). The sensitivity of this method makes it possible to monitor directly redox changes of el...

A new method for the production of boron nanoparticles is described. Boron trichloride is dissociated through injection into thermal plasma followed by a nucleation process producing boron nanoparticles. The ambient oxidation of the as-produced nanoparticles is also investigated. The nanoparticles were characterized with scanning transmission electron microscopy, electron energy loss spectrosco...

This study reports a green approach to synthesis of monometallic platinum nanoparticles (Pt NPs) and bimetallic aurium@platinum nanoparticles (Au@Pt) using aqueous leaf extract of Carica papaya as a reducing and stabilizing agent. The nature and morphology of as-synthesized PtNPs and bimetallic Au@Pt NPs were characterized using UV/vis spectroscopy (UV–vis), high resolution transmission electro...

A tetrasubstituted tetraferrocenylstannane is formed from 1-bromoferrocene-1'-carboxylic acid methyl ester and copper bronze. The molecular structure is almost perfectly tetrahedral with FeFe distances of around 6 A. In solution two sequential one-electron processes and one two-electron process are indicative of mixed-valent intermediates. Intermetallic interactions have been probed by preparat...

The phenomenon of fast electron channeling in atomic crystals has long been appreciated as an important factor in TEM characterization, being particularly critical for consideration in scanning transmission electron microscopy (STEM). As such, electron channeling effects have been examined to understand the thickness-dependence of annular-dark-field (ADF) STEM image contrast [1], the emergence ...

nickel hydroxide nanostructures were synthesized by a hydrothermal reaction. the effect of different precursors and surfactants on the morphology of nickel hydroxide nanostructures was investigated. nanostructures were characterized by x-ray diffraction, energy dispersive x-ray spectroscopy, scanning electron microscopy and fourier transform infrared  spectroscopy. the influence of ni(oh)2 nano...

Oxidative polymerization of aniline in aqueous solution in the presence of trehalose was conducted. Fourier transform infrared spectroscopy confirmed successful preparation of polyaniline containing a trace amount of trehalose. Electron spin resonance spectroscopy revealed that electron spin concentration of the polyaniline increases with aniline/trehalose ratio in the polymerization. Scanning ...