A LC method for corticosteroids (CC) determination in poultry feed using a Chromolith column and UV detection has been developed and validated. The method development involved the optimization of different hydro-organic mobile phases using methanol or ACN as organic modifiers, flow rate, and temperature. The optimum separation was achieved at 40 degrees C using ACN/water (21:79 v/v) as mobile p...

Monolithic silica spin column extraction (MonoSpin-SPE) was developed as a simple, sensitive, and eco-friendly pretreatment method which combined with ultra-fast liquid chromatography-mass spectrometry (UFLC-MS) to determine the levels of six phthalate esters, dimethyl-(DMP), diethyl-(DEP), dipropyl- [DPrP], butyl-benzyl-(BBP), dicyclohexyl(DcHP), and di- n-octyl-(DOP) phthalate in physiologica...

BACKGROUND Tylosin and Josamycin are macrolide antibiotics. They are used in the treatment of pneumonia, arthritis and mastitis in cattle, and mycoplasma infections in poultry. The incorrect use of antibiotics has lead to the presence of antibiotic residues in foods. The residues cause toxic effects on consumers. RESULTS A simple and sensitive method was optimized and validated for the analys...

Prefabricated beam–column connections are the most vulnerable components of prefabricated buildings during earthquake events. The seismic performance connection is functional as critical component plays a key role in structural safety. This study aimed to develop novel hybrid concrete (HPC) connection, combining with wet and dry techniques, enhance frames. A quasi-static experimental investigat...