Nanosize Nickel ferrite (NiF) was synthesized by the co-precipitation methods, and its effect as a 5% mass additive studied on thermal decomposition of micrometer nanometer size NTO. In presence NiF additive, peak temperature NTO decreased from 276.36 to 260.18 °C that nanoNTO 261.38 258.89 (β = 10 min−1). The kinetics parameters confirm catalytic activity for NTO, nNTO such activation energy (...