Graphene is a hot area of research because of its unique and remarkable properties. These properties have invoked researchers to use this form of carbon in various potential applications. One of the bottlenecks in developing such application is mass production of graphene. Hummer’s Method is one of the easiest and economical methods to synthesize huge amount of reduced graphene oxide (RGO) shee...

Certification of the phase compositions of the three NIST Reference Clinkers will be based upon more than one independent method. The current reference values were established using an optical microscope examination, with additional optical microscope data taken from an ASTM C 1356 round robin. The present X-ray powder diffraction (XRD) study provides the second, independent estimate of the pha...

To compare sample data from x-ray diffraction a suitable metric is developed to evaluate the similarity (or dissimilarity) between samples and to compare it to a references. The methodology focuses on the d-lines and uses the intensity measurements indirectly in the algorithm. The resulting d-line distribution and summary statistics of the differences is used to establish whether a true differe...

Nano-zeolite CoAPO-5 as a member of AFI family, was synthesized via a hydrothermal treatment, and structurally characterized using X-ray diffraction (XRD), scanning electron microscope (SEM), and energy dispersive X-ray analysis (EDAX). The effects of crystallization temperature and time on the structure of these powder products were studied. XRD patterns of the synthesized powders revealed a h...

Nano-zeolite CoAPO-5 as a member of AFI family, was synthesized via a hydrothermal treatment, and structurally characterized using X-ray diffraction (XRD), scanning electron microscope (SEM), and energy dispersive X-ray analysis (EDAX). The effects of crystallization temperature and time on the structure of these powder products were studied. XRD patterns of the synthesized powders revealed a h...

Certification of the phase compositions of the three NIST Reference Clinkers will be based upon more than one independent method. The current reference values were established using an optical microscope examination, with additional optical microscope data taken from an ASTM C 1356 round robin. The present X-ray powder diffraction (XRD) study provides a second, independent estimate of the phase...

we evaluated the effect of fe/alumina catalyst contained different cadmium contents and two synthesis temperatures on producing carbon nanotubes by chemical vapor deposition of methane as a feedstock.  x-ray powder diffraction (xrd), n2 adsorption-desorption, scanning electron microscopy (sem), transmission electron microscopy (tem), raman spectroscopy and thermogravimetry analysis (tga) were u...

in this work, we report on the synthesis of superparamagnetic iron oxide nanoparticles at room temperature using microemulsion template phase consisting of cyclohexane, water, ctab as cationic surfactant and butanol as a cosurfactant. surface modification have been carried out by using poly(ethyleneglycol) (peg). the structure,morphology, and magnetic properties of the products were characteriz...