نتایج جستجو برای: solvent free condition

تعداد نتایج: 857817  

Journal: :organic chemistry research 0
habib ollah foroughi department of scince, islamic azad university, fasa branch ali khalafi-nezhad department of chemistry, shiraz university, shiraz,71454, i.r.iran

the silica boron sulfuric acid nanoparticles (sbsans) as an efficient heterogeneous solid acid catalyst with both brønsted and lewis acidic sites catalyzed the preparation of bis-4-hydroxycoumarin derivatives using reaction of aldehydes and 4-hydroxycoumarin under mild and solvent-free condition at room temperature. this new and efficient methodology has advantages in comparison with currently ...

Journal: :iranian journal of catalysis 0
mohammad ali ghasemzadeh department of chemistry, qom branch, islamic azad university, qom, p.o. box 364/37185. i.r. iran. zahra elyasi department of chemistry, qom branch, islamic azad university, qom, p.o. box 364/37185. i.r. iran.

this study introduces a green and efficient method for preparation of biologically-active substituted 4h-pyrans using the one-pot three-component reaction of aromatic aldehydes, dimedone and malononitrile in the presence of cobalt oxide nanoparticles. co3o4 nanoparticles were used as an efficient catalyst for the synthesis of polyhydroquinoline derivatives by the reaction of aromatic aldehydes,...

Journal: :iranian journal of analytical chemistry 2014
maryam malekzadeh faeze daneshfar seyed mohsen sadeghzadeh

nano sio2/hyperbranched polyglycerol (hpg)/so3h catalyst was readily prepared for first time from inexpensive starting materials in aqueous media which catalyzed the synthesis of benzoic acid. ftir spectra, x-ray diffraction (xrd) and transmission electron micrographs (tem) was employed to characterize the properties of the synthesized nano sio2/hpg/so3h. high catalytic activity and ease of rec...

Journal: :iranian chemical communication 2015
mohammad ali nasseri ali allahresani batol zakeri nasab

microwave assisted green synthesis of α, ά- bis (substituted- benzylidene) alkanones by the crossed- aldol condensation reaction of substituted aryl aldehydes with ketones in the presence of catalytic amount of nbcl5 in good to excellent yields. this reaction is carried out under solvent-free conditions. the results showed that aldehydes bearing electron–donating substituent's on phenyl-ring fa...

Journal: :organic chemistry research 2016
hossein eshghi m eftekhar m rahimizadeh m hassanpour m bakavoli

cobalt hydrogensulfate is an efficient catalyst for the condensation of β-naphthol, aromatic aldehydes and 5,5-dimethyl-1,3-cyclohexanedione at 120 °c to afford 9,9-dimethyl-12-phenyl-8,10,11,12-tetrahydro-9-h-benzo[a]xanthen-11-one derivatives in high yields. also, polycondensation reactions of phenols with phthalic anhydride were carried out in the presence of cobalt hydrogensulphate under so...

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