The bulk SnO2 was synthesized by oxidizing the fine powder (50 mesh) of metallic tin (purity 99.99, Aldrich) powder at 750°C for 9 hrs hours in programmable temperature controlled furnace. The gross structure and phase purity of the powder sample ground from sintered pellets were examined by powder X-ray diffraction technique. The phase identification /gross structural characteristics of synthe...

CPD chairman’s message, Paolo Scardi 2 CPD projects: 2 Quantitative Phase Analysis RR, Ian Madsen Editor’s message, Robert Dinnebier 2 Thirty five years ago, Hugo Rietveld 3 WWW sites related to Powder Diffraction 5 IUCr Commission on Powder Diffraction 5 Rietveld Refinement from Powder Diffraction Data Beyond the abilities of Rietveld analysis: MEM-based pattern fitting with synchrotron X-ray ...

OBJECTIVE To compare the dissolution properties of Ginseng micropowder and common powder in vitro and investigate the effect of micronization on dissolution of Ginseng. METHODS Five ginsenosides including Rg1, Re, Rf, Rb1, and Rb2 were determined by high performance liquid chromatography, and the dissolution curves of Ginseng micropowder and common powder were drawn. RESULTS The dissolution...

Forty patients undergoing routine bronchoscopy were randomised to receive inhaled micronised gentamicin powder (180 mg) or nebulised gentamicin solution (160 mg) one hour before the procedure. Similar levels of gentamicin were detected in bronchoalveolar lavage fluid in the two groups (micronised powder (n = 20) 9.3 (SD 9.3) mg/l, nebulised solution (n = 20) 8.0 (7.8) mg/l). The micronised gent...

The objective of this study was to produce well-dispersed nanosized yttria tetragonally stabilized zirconia (Y-TZP) powder in aqueous suspension. The Y-TZP powder was produced by precipitation from homogeneous solution at 2001C under hydrothermal conditions. A homogeneous solution was created through the use of a complexing agent, which subsequently could be used in a dispersion scheme develope...

This study evaluated the effectiveness of dry Moringa oleifera leaf powder in the management of anaemia in adult albino rats. The proximate, mineral, vitamin and phytochemical composition of dry M. oleifera leaf powder were analysed. Twelve adult albino rats grouped into three were used. Cyclophosphamide was used to induce anaemia into them. The percentage proximate values were protein (26.28%)...

Single crystalline BaTiO3 (BT) was prepared using TiCl4, BaCl2 and oxalic acid. The structure of the prepared nanocrystalline BT powders were a tetragonal perovskite according to XRD and HRTEM analysis. Annealing powder to 750C show that pure BT phase was formed according to XRD, TG, and FTIR spectroscopy. The TEM images of the prepared powder reveal spherical morphology of BT, while a finger t...

Three variations of tomato fudge were prepared using tomato powder at different proportions with sugar, whole milk and honey and evaluated for sensory quality, antioxidant activity, microbial count and consumer acceptability. It was observed that the fudge prepared by using 1-3 g of tomato powder were having higher sensory scores while antioxidant activity was found highest in fudge having 5 g ...

A powder library of layered Li(Ni,Co,Ti)O2 (Ni ≤ 0.8, Ti ≤ 0.2) compounds was prepared by electrostatic spray deposition. From powder x-ray diffraction patterns, most of the powder library sintered at 700 ○C was indexed as a single phase belonging to the space group R[Formula: see text]m. These results were almost identical to those obtained from a study by combinatorial exploration. We investi...

Properties of TiO2 powder got hydrometallurgically from the slag that was, together with pig iron, a product of reductional red mud electromelting were investigated using physico-chemical methods of analyzing. The samples of TiO2 powder contain high quantity of titanium compared with the used raw material granulated slag. Investigating the mophology of the powder samples, it has been found out ...