Influence of pulse modulation of the coil current sustaining a high-power Ar-N2-H2 induction thermal plasma was experimentally studied on the time-averaged particle composition of the thermal plasma. Optical emission spectroscopy measurement was carried out to obtain the time evolution in the relative radiation intensities of excited atoms and molecules flowing into the reaction chamber. The ra...

in a hydrothermal route devoted for synthesis of ca10(po4)6(oh)2 (ha) nanostructures, morphology can be controlled by experimental condition to form magical ha or nanostructured nanoparticles. in an intermediate condition, a novel nanostructure namely rose-like bundle of ha rod-likes was found, which is different from known ha nanostructures. the chemical synthesis of nanopowders under hydrothe...

We compared five ion-selective electrodes (ISEs; AVL 985S, Baxter Lytening 2Z, Beckman EL-ISE, Ciba-Corning 654 Na/K/Li, and Nova CRT 11) and a colorimetric method (Ektachem) for determination of lithium with flame atomic absorption and atomic emission spectroscopy. We evaluated precision, recovery, interference by drugs (procainamide, N-acetylprocainamide, quinidine, lidocaine, carbamazepine, ...

Spectroscopy of planetary nebulae (PNe) provides the means to investigate s-process enrichments of neutron(n)-capture elements that cannot be detected in asymptotic giant branch (AGB) stars. However, accurate abundance determinations of these elements present a challenge. Corrections for unobserved ions can be large and uncertain, since in many PNe only one ion of a given n-capture element has ...

The design of active and stable semiconducting composites with enhanced photoresponse from visible light to near infrared (NIR) is a key to improve solar energy harvesting for photolysis of water in photoelectrochemical cell. In this study, we prepared earth abundant semiconducting composites consisting of iron pyrite and Titanium oxide as a photoanode (FeS2/TiO2 photoanode) for photoelectroche...

Urbanization, industrialization and other human activities has introduced a number of heavy metal contaminants in the environment. Microorganisms inhabiting such sites are well efficient in developing resistance strategies against toxic heavy metal stress. The present work qualitatively describes uptake of nickel (Ni) and lead (Pb) by epiphytic root bacteria isolated from the rhizosphere of the...

the knoevenagel condensation of aromatic aldehydes with barbituric acid, dimedone and malononitrile occurred in the presence of bf3/nano-γ-al2o3 at room temperature in ethanol. this catalyst is characterized by powder x-ray diffraction (xrd), fourier transform infrared spectroscopy (ft-ir), thermal gravimetric analysis (tga), field emission scanning electron microscopy (fesem) and energy-disper...

This article presents the method of extraction-preconcentration of Lead, Cadmium, and Nickel ions from food samples using the Ghezeljeh montmorillonite nanoclay (Geleh-Sar-Shoor) as a new native adsorbent in batch single component systems. The extractionpreconcentration of heavy metals were carried out by applying the solid phase extraction (SPE) method followed by atomic absorption spectroscop...