mgcl2/c2h5oh adducts with constant relative ratio of 1/3 were prepared and kept at 120oc for different lengths of times of 5, 10, 20, 30, 50, 90,120 and 220 h. then the samples were quenched and analyzed by xrd and bet. no meaningful changes were observed in the specific surface area of the samples, while xrd spectra showed 3 peaks at 2θ<15o for samples kept at 120oc for 5 h. these 3 peaks were...

S-doped and bare mesoporous TiO2 were prepared using titanium tetraisopropoxide and thiocarbamide as raw materials. Prepared materials were characterized by means of fourier transform infrared spectroscopy FT-IR, thermogravimetry-differential scanning calorimetry (TG-DSC), X-ray diffraction (XRD), UV–Vis absorption spectroscopy, Brunauer–Emmett–Teller (BET) specific surface area and Barrett–Joy...

Using Fe(NO3)3.9H2O, Co(NO3)2.6H2O and Mn(NO3)2.4H2O the magnetic properties of nanoparticles trimetalic Iron - Cobalt - Manganese, with supported Magnesium oxide have been prepared by Co-precipitation and Solvothermal methods. The prepared samples are characterized by Scanning Electron Micros...

Objective(s): Lead is a very strong poison in the environment. Lead toxicity can be affected on the human body and caused disease. Therefore, the design of lead sorbent can be had the great help to the medical field. In this work, the nanohydroxyapatite (n-HA) was used for removal of lead from aqueous solution. Then, polycaprolactone (PCL) nanocomposite was modified with n-HA by simple preparat...

In this paper, xCuO/CeO2–γAl2O3 nano-catalysts were successfully synthesized by precipitation from an aqueous solution which modified via ultrasonic waves. For characterization of xCuO/CeO2–γAl2O3 samples N2 adsorption results showed that the BET surface area of the CuO/CeO2–γAl2O3, X-ray diffraction (XRD), scanning electron microscope (SEM) and energy dispersive X-rays (EDX dot-mapping) were u...

Toluene and benzene were eliminated using multi-walled carbon nanotubes (MWCNTs). In order to investigate influence of acid treatment on the MWCNTs adsorption capacities, the MWCNTs were functionalized by nitric acid (10 M) under reflux conditions for 2 h. Fourier transform infrared (FTIR) and Raman spectroscopy were employed to confirm the formation of functional groups on the nanotubes su...

Powder activated carbon surface (AC) was grinded and modified and altered procedure thorough a facile and easy chemical reaction to appearance of 2-((3silylpropylimino)1-methyl) phenol (AC- (SPIMP)). Subsequently, this novel sorbent efficiently applied for the extraction and preconcentration of some metal ions from real samples. Preliminary the influences of variables such as pH, amounts of rea...

In this study, granular activated carbon, GAC, was modified by oxidation with H2O2 and NaClO aqueous solutions and heat treatment at 900 °C. The N2 adsorption isotherms at −196 °C and SEM and FTIR results were used to characterize the properties of the prepared ACs. Textural parameters such as BET surface area and pore volumes were assessed by gas adsorption. The BET surface area values of soli...

Unlike most conventional anode materials, the newly developed TiNb2O7 (TNO) does not form a solid electrolyte interface (SEI) layer, which makes it safe for high power requiring lithium-ion batteries. In this paper, we demonstrated an SBA-15 confined synthetic approach to prepare TNO nanoparticles (S-TNO) with a small particle size around 10 nm and a large BET surface area of 79.5 m(2) g(-1). I...

The spray-pyrolysis of borazine at 1400 °C under nitrogen generates boron nitride (BN) nanoparticles (NPs). The as-prepared samples form elementary blocks containing slightly agglomerated NPs with sizes ranging from 55 to 120 nm, a Brunauer-Emmett-Teller (BET)-specific surface area of 34.6 m g and a helium density of 1.95 g cm. They are relatively stable in air below 850 °C in which only oxidat...