In this paper, a characterization of an AlSiMg alloy processed by direct metal laser sintering (DMLS) is presented, from the analysis of the starting powders, in terms of size, morphology and chemical composition, through to the evaluation of mechanical and microstructural properties of specimens built along different orientations parallel and perpendicular to the powder deposition plane. With ...

deep cryogenic heat treatment is assumed as a supplementary heat treatment performed on steels before the finaltempering treatment to enhance the wear resistance and hardness of the steels. in this study, the effects of thedeep cryogenic heat treatment on the wear behavior and corrosion resistance of the 1.2080 tool steel were studiedusing the wear testing machine and polarization and impedance...

We report the synthesis and characterization of mesostructured thin silica films derived from methyltriethoxysilane (MTES) and/or tetraethyl orthosilicate (TEOS) silica precursors and polystyreneblock-poly(ethylene oxide) (PS-b-PEO) diblock copolymers via the solvent evaporation-induced self-assembly (EISA) process. It is found that the mesoand microstructure of the calcined films consists of c...

The recent development on TEM work of irradiated RERTR fuels includes characterization of the irradiated U-10Mo/Alloy-6061 monolithic fuel plate, the RERTR7 U-7Mo/Al-2Si and U-7Mo/Al-5Si dispersion fuel plates. It is the first time that a TEM sample of an irradiated nuclear fuel was prepared using the focused-ion-beam (FIB) liftout technical at the Idaho National Laboratory. Multiple FIB TEM sa...

We present an in situ approach for the characterization of lithium intercalation/deintercalation in thinfilm Li-ion battery electrodes. The method allows simultaneous measurement of microstructural changes during lithiation using micro-Raman (mRaman) spectroscopy in parallel with stress changes via optical interferometry. We observe evolution in the microstructure and stress in the various crys...

Al-doped ZnO (AZO) and In-doped ZnO (IZO) nanopowders were prepared by a sol-gel route and subsequent drying in ethanol under supercritical conditions. The morphological and microstructural properties were investigated by transmission electron microscopy (TEM) analysis and X-ray powder diffraction (XRD). The characterization study showed that the AZO and IZO nanoparticles were crystalline and e...

In continuation with our studies concerning the synthesis, characterization and biological evaluation of nucleolipidic Ru(III) complexes, a novel design for this family of potential anticancer agents is presented here. As a model compound, a new uridine-based nucleolipid has been prepared, named HoUrRu, following a simple and versatile synthetic procedure, and converted into a Ru(III) salt. Sta...

This study involves the preparation, microstructural, physical, mechanical and biological characterization of novel gelatine and gelatine/elastin gels for their use in the tissue engineering of vascular grafts. Gelatine and gelatin/elastin nanocomposite gels were prepared via a sol-gel process, using soluble gelatine. Gelatine was subsequently crosslinked by leaving the gels in 1% glutaraldehyd...

Microstructural characterization of plutonium by electron backscattered diffraction (EBSD) has been previously elusive primarily because of the extreme toxicity and surface oxidation rates associated with plutonium metal. In this work, initial electron backscattered diffraction pattern (EBSP) observations of a plutonium-gallium (Pu-Ga) alloy were made. Samples were prepared using standard metal...