نتایج جستجو برای: microwave assisted

تعداد نتایج: 176049  

Curcumin is a natural bioactive compound originated from the rhizomes of turmeric (Curcuma longa L.). This study was performed to investigate formic acid and microwave assisted extraction of curcumin from turmeric (Curcuma longa L.). In order to enhance the curcumin extraction, different parameters such as particle size, effect of pretreatment with water, radiation intensity and type of solvent...

2011
Kazuo Katoh

Microwave irradiation during tissue fixation and immunostaining reduces the sample preparation time. Microwave irradiation also facilitates the penetration of fixatives and antibody solutions into the tissues, resulting in efficient fixation and reduction of non-specific antibody binding, respectively. Experimental procedures involving immunofluorescence microscopy are time-consuming as this me...

Journal: :Ultrasonics sonochemistry 2015
Meryem Boukroufa Chahrazed Boutekedjiret Loïc Petigny Njara Rakotomanomana Farid Chemat

In this study, extraction of essential oil, polyphenols and pectin from orange peel has been optimized using microwave and ultrasound technology without adding any solvent but only "in situ" water which was recycled and used as solvent. The essential oil extraction performed by Microwave Hydrodiffusion and Gravity (MHG) was optimized and compared to steam distillation extraction (SD). No signif...

2015
Bai-Liang Xue Jia-Long Wen Run-Cang Sun

Lignin-based polyols were synthesized through microwave-assisted liquefaction under different microwave heating times (5-30 min). The liquefaction reactions were carried out using polyethylene glycol (PEG-400)/glycerol as liquefying solvents and 97 wt% sulfur acid as a catalyst at 140 °C. The polyols obtained were analyzed for their yield, composition and structural characteristics using gel pe...

2012
Shigenori Togashi

A pilot plant for continuous flow microwave-assisted chemical reaction combined with microreactors was developed and water heating tests were conducted for evaluation of the developed plant. We developed a microwave apparatus having a single microwave generator that can heat reaction solutions in four reaction fields simultaneously in order to increase throughput. We also designed a four-branch...

Journal: :Journal of the American Society for Mass Spectrometry 2005
Shan-Shan Lin Chi-Hong Wu Mei-Chuan Sun Chung-Ming Sun Yen-Peng Ho

The work describes the accelerated enzymatic digestion of several proteins in various solvent systems under microwave irradiation. The tryptic fragments of the proteins were analyzed by matrix-assisted laser desorption/ionization mass spectrometry. Under the influence of rapid microwave heating, these enzymatic reactions can proceed in a solvent such as chloroform, which, under traditional dige...

Ashraf S. Shahvelayati Jila Vesalian

Benzylaminoalkenones and benzylaminoalkenoates 3 were synthesized from reaction of benzylamine with corresponding 1,3-diketones and 1,3-ketoesters in the presence of catalytic amount of chloroacetic acid under microwave radiation. This method offers several advantages including high yield of products, recyclable of the catalyst and easy experimental work-up procedure.

In the present work, we have developed a mild, efficient, and environmentally benign method for the synthesis of tetrahydrobenzo[b]pyran derivatives via a three-component cyclocondensation of aldehydes, malononitrile and dimedone utilizing ammonium chloride as a simple, easily available and cost effective catalyst under microwave irradiation. This method has several attracting features such as ...

Journal: :پژوهش های علوم و صنایع غذایی ایران 0
mohsen gavahian reza farhoosh asgar farahnaky katayoun javidnia fakhri shahidi

as traditional extraction methods like hydrodistillation (hd) and steamdistillation (sd) have long extraction times, some novel extraction methods like microwave-assisted hydrodistillation (mahd) and ohmic-assisted hydrodistillation (oahd) are recently introduced. in this study, essential oils of mentha piperita were extracted by oahd and mahd and the results were compared with those of the sd ...

2016
Michael Antony Samy Amutha Gnana Arasi Manchineela Gopal Rao Janardanan Bagyalakshmi

Introduction: Fruit polysaccharides, essential health factors in foods, are widely present in edible fruits. Several methods for isolation of polysaccharide are available. Microwave Assisted Extraction (MAE) method is extensively used for separation of polysaccharides. Only little information is available about Psidium guajava L. Fruit Polysaccharide (PFP) and its extraction methods. Objective:...

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