Orientated ferromagnetic Ni0.89Fe0.11 nanoparticle/polymer nanofibres were made by electrospinning a solution containing iron(III) nitrate nonahydrate, nickel(II) acetate tetrahydrate, polyvinylpyrrolidone, and acetic acid in methanol thermally processed Ar then 95%Ar:5%H2 up to 620 °C. There was distribution nanofibre widths after with wider (average width 440 nm) some thinner 120 nanofibres. ...