نتایج جستجو برای: solvent free microwave extraction

تعداد نتایج: 758549  

Journal: :Materials advances 2022

Carbon dots were synthesized using solvent-free, microwave synthesis and photoreduction of methyl viologen was studied under visible wavelength light irradiation.

Journal: :Molecules 2010
Siham Mallouk Khalid Bougrin Abdelaziz Laghzizil Rachid Benhida

A sustainable Knoevenagel condensation of a series of aldehydes with malononitrile and ethyl cyanoacetate is described. The process is based on the combination of microwave activation and hydroxyapatite catalysis under solvent-free conditions. Products are obtained in and high yields after short reaction times. The effects of the specific surface of porous calcium hydroxyapatite and microwave a...

2014
Forough Ghasemi Naghdi Skye R. Thomas-Hall Reuben Durairatnam Steven Pratt Peer M. Schenk

*Correspondence: Peer M. Schenk, Algae Biotechnology Laboratory, School of Agriculture and Food Sciences, The University of Queensland, Level 5, John Hines Building, Brisbane, QLD 4072, Australia e-mail: [email protected] Microalgal lipid recovery for biodiesel production is currently considered suboptimal, but pre-treatment of algal biomass, the use of solvent mixtures and the positioning of ...

Multicomponent condensation of 1-naphthol, malononitrile, and arylglyoxals in the presence of Mg-Al hydrotalcite under solvent-free MicroWave (MW) conditions gave a new series of 2-amino-4-aroyl-4H-benzo[h]chromene-3-carbonitriles in high yields (70-89%). The structure of all products was elucidated by their...

2007
Luiza Găină Castelia Cristea Claudia Moldovan Dan Porumb Emanoil Surducan Călin Deleanu Abdalah Mahamoud Jacques Barbe Ioan A. Silberg

Application of a dynamic microwave power system in the chemical synthesis of some phenothiazine and quinoline derivatives is described. Heterocyclic ring formation, aromatic nucleophilic substitution and heterocyclic aldehydes/ketones condensation reactions were performed on solid support, or under solvent free reaction conditions. The microwave-assisted Duff formylation of phenothiazine was ac...

2015

Jatropha curcas has a variety of uses which are of great economic significance. Jatropha oil can be used as fuel alternative and for making biodiesel that is supposed to overcome the source limitation problem. In this study, conventional, ultrasound assisted and microwave pretreatment solid liquid extraction of Jatropha seed were studied in terms of amount and quality of the extracted oil. The ...

Journal: :Molecules 2007
Michal Neuschl Darek Bogdal Milan Potacek

New compounds with the ethyl hexahydro-1H-pyrrolo[3,2-c]quinoline-2-carboxylate skeleton were prepared by microwave-assisted intramolecular 1,3-dipolar cycloaddition reactions. The reactions were carried out under solvent-free conditions and compared with the same reaction in the presence of a solvent and a catalyst. Steric effects on the selectivity of the reaction were noted and evaluated.

2011
R. Thomas R. Tripathi S. D. Kamat D. V. Kamat

The extraction of active compounds from plants is one of the most critical steps in the commercial development of natural products for medicinal and health benefits. In view of the large number of plant species potentially available for study, it is essential to have efficient systems for the rapid and efficient extraction of phytochemicals for further investigation on their properties. The pre...

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