The separation of tetracyclines (TCs) using reversed-phase liquid chromatography (LC) is proposed. The use of an amide-based stationary phase prevents the interaction of tetracyclines with the residual silanol groups and thus avoids the appearance of tailed peaks. Detection was based on using an UV spectrophotometer and gradient elution with acetonitrile-oxalic acid as mobile phase permitted go...

In this report, ZnO nanoparticles (NPs) was synthesized by chemical method using Zinc Acetate dehydrate [Zn(CH3COO)2.2H2O)] as precursors and Ethanol distilled water solvent. Sodium hydroxide (NaOH) used to maintain the pH helps establish NPs. The NPs are characterized XRD, UV-visible spectroscopy SEM image analysis. XRD characterization gives polycrystalline nature of with size ~23 nm ~27 calc...

Magnetized water showed alterations in the electrolyte potential and vibration modes. This study aimed to investigate the effect of magnetic water and physiological solutions on the UV-spectra of tramadol HCl. Distilled water as well as full strength or diluted physiological solutions are magnetized by magnetic disc. Then tramadol HCl was dissolved in each magnetic and in non-magnetic solution ...

The thiobarbiturates differ from other barbiturates in having a sulfur atom in place of the carbonyl oxygen at the C-2 position. The drug 2-thiobarbituric acid was found to be sufficiently soluble in 95% ethanol and 5% water for highly sensitive detection and assay. Analytical samples, including standards, were studied at 320 nanometer wavelength with background absorbance of the solvent correc...

Measurement of the UV-visible absorption spectrum is a convenient technique for detecting chemical changes of proteins, and it is therefore useful to combine spectroscopy and diffraction studies. An online microspectrophotometer for the UV-visible region was developed and installed on the macromolecular crystallography beamline, BL38B1, at SPring-8. This spectrophotometer is equipped with a dif...

Vanadium supported on highly ordered nanoporous silica (VOxLUS-1) was synthesized and characterized by XRD, Nitrogen adsorption desorption isotherms and UV-visible spectrophotometer. Direct oxidation of benzene to phenol in liquid phase by H2O2 peroxide was examined by using various solvents (methanol, acetone, acetic acid, acetonitryl). The maximum yield (25%) and selectivity (73%) of the phen...

In this study, the effects of some environmental storage conditions – light, temperature and humidity on the stability of the steroidal drug, hydrocortisone sodium succinate injection were investigated. The drug samples were stored at varying conditions of light, temperature (0C, 28C and 60C) and humidity, after which each sample was assayed at weekly intervals for their content of the drug usi...

This experimental study aimed to compare the adsorption of oleic acid (fatty acid) by two adsorbent; activated carbon and carbon nanotube by use of Uv-Vis spectrophotometer Jenway 6505 model. In this study, five different concentrations of oleic acid in the range of 282.47ppm to 847.41ppm were used. In all conducted experiments, the values of adsorbents, exposure time, temperature, and pH were ...

Thin and transparent films of doped cadmium sulfide (CdS) were obtained on commercial glass substrates by Chemical Bath Deposition (CBD) technique. The films were doped with low concentration of Sn, and annealed in air at 300 °C for 45 min. The morphological characterization of the films with different amounts of dopant was made using SEM and EDAX analysis. Optical properties of the films were ...

Affinity separation with magnetic beads is an important and widely used technique for DNA computing. We have designed and implemented an experimental lab-on-a-chip module for affinity-bead separation for DNA-based concept learning. Magnetic beads with DNA-probe sequences immobilized on their surface were used to select target strands, and these beads are restrained in the channel by a permanent...