: We have studied the effects of shutter transients (STs) in molecular beam epitaxy (MBE). Two series of samples were grown by MBE and evaluated by X-ray diffraction (XRD) and X-ray reflectivity (XRR) measurements. The effects of STs were evaluated by growth rate (GR) analysis using a combination of growth time (GT) and thickness evaluated by XRD and XRR measurements. We revealed two opposite e...

The morphology and structure of 2,2':6',2″-ternaphthalene (NNN) deposited on muscovite mica(001) substrates was investigated by scanning force microscopy (SFM) and specular X-ray diffraction measurements. Consistently, both methods reveal the coexistence of needle-like structures with a {111} contact plane and {001} orientated island-like crystallites, which are built up by almost upright stand...

The characterization of iron thin films grown at different substrate temperatures has been performed by x-ray diffraction (XRD) and extended x-ray absorption fine structure (EXAFS). The film growing of iron at low temperatures provides an excellent system to test the results obtained from both techniques because the crystallographic grains present a variation of size and shape as a function of ...

During last decade, nanotechnology has gained a significant relevance in many areas of basic research and applied science. One of the great challenges in the field of nanotechnology is preparation of nanoparticles and nanostructures where new, not ordinary materials are used. In the present study, we observed self organizing structures prepared by the gas deposition method in N2 atmosphere. Gla...

An in situ time-resolved X-ray diffraction (XRD) system for hydrothermal reaction has been developed in order to investigate the phase evolution during autoclave process in autoclaved aerated concrete (AAC) formation. The system includes a novel autoclave cell for transmission XRD with thin beryllium windows, a two-dimensional photon-counting pixel array detector, and uses high energy X-rays fr...

Samples of CoFe2-xCrxO4 where x varies from 0.0 to 0.5 were prepared by co-precipitation route. These samples were sintered at 750°C for 2 hours. These particles were characterized by X-ray diffraction (XRD) at room temperature. The FCC spinel structure was confirmed by XRD patterns of the samples. The crystallite sizes of these particles were calculated from the most intense peak by Scherrer f...

Zn nanoparticles were prepared by the inert-gas evaporation technique with induction heating method. Asprepared Zn particles were mixed with Na2S solution. ZnS nanoparticles were synthesized under ultrasonic radiation. They were studied by X-ray diffraction (XRD), transmission electron microscopy (TEM), UV spectrophotometry, and X-ray photoelectron spectrometry (XPS). XRD revealed that the ZnS ...

In this letter, we report on the obtention of hafnium oxide (HfO2) nanostructures by the microwavehydrothermal method. These nanostructures were analyzed by X-ray diffraction (XRD), field-emission gum scanning electron microscopy (FEG-SEM), transmission electron microscopy (TEM), energy dispersive X-ray spectrometry (EDXS), ultraviolet–visible (UV–vis) spectroscopy, and photoluminescence (PL) m...

We present a transmission electron microscopy ~TEM!/Rutherford backscattering spectrometry ~RBS!/x-ray-diffraction ~XRD! study of Au evaporated on crystalline organic thin films of diindenoperylene ~DIP!. Cross-sectional TEM shows that the preparation conditions of the Au film ~evaporation rate and substrate temperature! strongly determine the interfacial morphology. In situ XRD during annealin...

The corrosion inhibition of mild steel in 0.5 M H2SO4 solution has been investigated using electrochemical methods, X-ray diffraction (XRD) and scanning electron microscope (SEM). The adsorption and inhibition action of acid corrosion of mild steel using cetyltrimethylammonium bromide (CTABr) and different halides (NaCl, NaBr and NaI) has shown synergetic effect. The results showed that the pro...