نتایج جستجو برای: accelerated solvent extraction
تعداد نتایج: 273883 فیلتر نتایج به سال:
Hexane, the common solvent for extraction of edible oils from seeds is no more considered safe due to the presence of solvent in oil and also solvent vapour, a hazardous air pollutant. We have carried out the experiments with bahera (Terminalia bellerica Roxb) and flax seed (Linum usitatissimum ) oil as these oils are highly used in food for their nutraceutical values. The extraction of edible ...
Hot-water extraction of hemicelluloses, especially galactoglucomannans, from fractions of ground spruce wood with different particle sizes was studied at 170°C with extraction times up to 60 min. Extraction of spruce sapwood, heartwood, and thermomechanical pulp (TMP) was also compared at 160 to 180°C. Static batch extractions were carried out in an accelerated solvent extractor (ASE). The extr...
modified bubble column extraction with ultrasonic bath (bce-ub) method was used to extract atropine from the stem and leaves of atropa belladonna. optimum condition were obtained with kamada solvent which was chloroform-methanol-ammonia 15:15:1(v/v/v) as extraction solvent, the particle size of less than 350 µm, an extraction time of 23.95 min, a liquor to material ratio of 15.08 ml/g and an...
Oilseeds are crucial for the nutritional security of the global population. The conventional technology used for oil extraction from oilseeds is by solvent extraction. In solvent extraction, n-hexane is used as a solvent for its attributes such as simple recovery, non-polar nature, low latent heat of vaporization (330 kJ/kg) and high selectivity to solvents. However, usage of hexane as a solven...
a simple, rapid and sensitive solvent assisted-dispersive solid phase extraction method was developed for the extraction of iron(ii) prior to its spectrophotometric determination. the fe(ii) reacted with 2,4,6-tris(2-pyridyl)-1,3,5-triazine, neutralized with sodium dodecyl sulfate and extracted onto the fine particles of benzophenone which were formed upon rapid injection of a mixture of benzop...
We present an improved method for ultraviolet spectrophotometry of theophylline in serum. We studied various extraction techniques aimed at eliminating interferences from co-extractable serum constituents. In the resulting modified procedure, 1 ml of serum is required and a salt-solvent pair of ammonium sulfate and chloroform/hexane is used for extraction. The solvent forms the top phase after ...
In the proposed method, carbon tetrachloride and ethanol were used as extraction and dispersive solvents. Several factors that may be affected on the extraction process, such as extraction solvent, disperser solvent, the volume of extraction and disperser solvent, pH of the aqueous solution and extraction time were optimized. Under the optimal conditions, linearity was maintained between 1.0 ng...
In the last 10 years there has been an increased interest in using techniques involving microwave-assisted extraction and pressurised solvent extraction in analytical laboratories. This review gives a brief overview of both methods, and reports on their application to the extraction of natural products. The influence of parameters such as the nature of the solvent and volume, temperature, time ...
Phenol was extracted from sebacic acid wastewater (SAWW) using liquid-liquid extraction in batch as well as serial modes by applying different solvent: SAWW (1:250 5:250, v/v). Alcohols (1-hexanol, 1-heptanol, and 1-octanol), castor oil and Aliquat-336® were used for phenol extraction. In a typical extraction experiment involving shaking and allowing for phase separation, phenol (75-96%) can be...
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