نتایج جستجو برای: crystal x
تعداد نتایج: 759426 فیلتر نتایج به سال:
Photocatalysis has attracted significant attention as a potential issue for the degradation of toxic organic pollutants such as Congo Red. In this research spherical Pure ZnO nano particles and Ni-Co-ZnO nano composites (Zn0.95Ni0.04Co0.01O, Zn0.95Ni0.025Co0.025O and Zn0.95Ni0.01Co0.04O) have been synthesized by precipitation method. X- ray diffraction, Fourier transform Infra Red ,field emis...
The copper(II) complex [Cu(pic)2]·2H2O was synthesized with 2-picolinic acid (Hpic) and copper acetate as reactants by room temperature solid-solid reaction. The composition and structure of the complex was characterized by elemental analyses, single crystal X-ray diffraction, X-ray powder diffraction, FT-IR spectroscopy and thermogravimetry-differential scanning calor...
Development of components that can form large molecular aggregates through non–covalent interactions, in nano size structures, has been an active area of research. In current study, a nano-sized Pb(II) coordination polymer, {[Pb(pydc)(pydc.H2)(H2O)2]2}n (1), where [pydc.H2= 2,6-pyridinedicarboxylic acid), wer...
In this study, encapsulated ZnO nanorods with different amount of chromium (Cr) dopant (0-4.5 at.%) were prepared with hydrothermal method, and their sensitivities as gas sensors against ethanol vapor were investigated. Morphologies of samples were explored by field emission scanning electron microscope (FESEM) which showed that encapsulation process increased the diameter of ZnO nanorods. Exis...
X-ray crystallography is an important method for determination of the arrangement of atoms within a crystal of compound in which a beam of X-rays strikes a crystal and causes the beam of light to spread into many specific directions. From electron density, in the molecule the mean positions of the atoms in the crystal can be determined, as well as their chemical bonds and various other informat...
First principle calculations of periodic crystal structure were successfully combined with powder X-ray diffraction measures to determine the structure of orotaldehyde monohydrate. This approach was particularly helpful to overcome the inadequacy of powder X-ray diffraction to reliably locate the hydrogen atoms of the intermolecular bond network of the crystal molecules. Density functional calc...
We report on the design and performance of a wavelength-dispersive type spectrometer based on the von Hamos geometry. The spectrometer is equipped with a segmented-type crystal for x-ray diffraction and provides an energy resolution in the order of 0.25 eV and 1 eV over an energy range of 8000 eV-9600 eV. The use of a segmented crystal results in a simple and straightforward crystal preparation...
X-ray diffraction from crystal surfaces at grazing angles gives rise to X-ray standing waves above and below the surface. Expressions are derived for the fluorescence observed from atoms located on or in a crystal as a result of excitation by the grazing-angle X-ray standing waves. In addition to the dependence of the fluorescence on the position of the atom with regard to the crystal plane tha...
Through the complementary use of single-crystal X-ray diffraction and X-ray absorption spectroscopy, we present in this paper the first direct results on the site occupancy of thorium in the fluorapatite structure and the structural distortion created by its substitution. Structure refinements based on single-crystal X-ray diffraction data from synthetic Th-doped fluorapatite indicates that Th ...
Red transparent single crystals of Ba9[NbN4]2O[CN2] were synthesised by the reaction of BaO coated Ba metal, C and Nb powder in arc-welded Nb ampoules at 1300 K. The title compound was characterised by X-ray single crystal diffraction (P1̄, a = 799.05(2), b = 962.61(2) and c = 1264.38(4) pm; α = 75.859(1), β = 85.745(1) and γ = 87.8621(8)◦; Z = 2) and Raman spectroscopy (νsym = 1234 and δ = 632/...
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