Ethylene glycol ingestion, accidental or intentional, can be a life-threatening emergency. Assays are not available from most clinical laboratories, and, thus, results often require many hours or days to obtain. Enzymatic assays, adaptable to automated chemistry analyzers, have been evaluated, but they have been plagued by analytic problems. With an alternative method of data analysis applied t...

The pharmacotherapy for Alzheimer's disease (AD) includes the use of acetylcholinesterase inhibitors (AChEI). Recent investigations for novel AD therapeutic agents from plants suggested that Tabernaemontana genus is a promising source of novel anticholinesterasic indole alkaloids. In this work two fast screening techniques were combined in order to easily identify novel cholinesterase inhibitor...

The aim of the present study was to investigate the various chemical components present in the volatile oil of the leaf of Cupressus torulosa and to find variation of essential oil components among the populations. Twenty-two, 17 and 20 compounds were identified with 95.45, 95.45 and 91.45% in Kalsi, Joshimath and Jeharikhal, respectively were identified by gas chromatography-mass spectrometry ...

N-nitrosamines are a class of carcinogenic chemical compound. Considering the large-scale application agrochemicals globally, elimination from pesticides should be priority for manufacturers and regulators. A set methods was developed validated determination toxicologically relevant N-nitrosamine impurity ethalfluralin (ethyl-N-(2-methylallyl) N-nitroso amine—EMANA) in 33% w v−1 emulsifiable co...

the leaves of four cultivated eucalyptus species, eucalyptus microtheca var. microtheca f. muell., eucalyptus spathulata, eucalyptus largiflorens and eucalyptus torquata were collected in spring from kashan and isfahan provinces (central region of iran). after drying the plant materials in shade, their essential oils were obtained by hydro-distillation. the oils were analyzed by capillary gas c...

Acrylates have been widely used in the synthesis of pharmaceutical polymers. The quantitation of residual acrylate monomers is vital as they are strong irritants and allergens, but after polymerization, are relatively inert, causing no irritation and allergies. Poly(ethylene oxide) (PEO) hydrogels were prepared using pentaerythritol tetra-acrylate (PETRA) as UV crosslinking agent. A simple, acc...

Cerebrospinal fluid (CSF) from uninfected patients and from patients with bacterial and viral meningitis was analyzed by gas-liquid chromatography, with use of a flame ionization detector, and by gas chromatography-mass spectrometry. The resulting profiles were consistent and reproducible. Hydroxy acids were the compounds found in greatest abundance in both normal and infected CSF. Control expe...

Exhaust particulate from compression ignition (CI) engines running on engine and chassis dynamometers was studied. Particulate dichloromethane extracts were qualitatively and quantitatively analyzed for polycyclic aromatic hydrocarbons (PAHs) and biomarkers by gas chromatography with flame ionization detector (GC-FID) and gas chromatography-mass spectrometry (GC-MS). PAH group profiles were mad...

the aim of this study was evaluation of phytochemical components, antioxidant activity, and antibacterial effects of basil (ocimum basilicum l.) essential oil (beo) in vitro. the lipid oxidation of the meat and antibacterial effects of beo were also evaluated in beef burger product. in this empirical study, essential oil of the basil was isolated by hydrodistillation. then, beo was analyzed by ...

This study reports, for the first time, chemical composition and biological activity of essential oil from Brazilian Cymbopogon densiflorus flowers. Thirty compounds were identified by gas chromatography coupled with mass spectrometry (GC/MS), corresponding to 95 % total an chromatogram obtained chromatography-flame ionization detection (GC-FID ). The was mainly composed cis-p-mentha-1(7),8-die...