Epoxy/Single Walled Carbon Nanotube Nanocomposite Thin Films for Composites Reinforcement. (May 2009) Graham Leicester Warren, B.S., Texas A&M University Chair of Advisory Committee: Dr. Hung-Jue Sue This work is mainly focused upon the preparation, processing and evaluation of mechanical and material properties of epoxy/single walled carbon nanotube (SWCNT) nanocomposite thin films. B-staged e...

The presence of thermal mismatch between different materials of plastic IC packages was found to cause reliability and moldability issues such as delamination and warpage phenomenon. Delamination and warpage between the mold compound and die attach adhesive material were evaluated for Quad Flat No-lead (QFN) package. Evaluation was conducted on two set of different materials combination of epox...

Toughening an epoxy resin by bio-based modifiers without trade-offs in its modulus, mechanical strength, and other properties is still a big challenge. This paper presents an approach to modify epoxy resin with tannic acid (TA) as a bio-based feedstock. Carboxylic acid-modified tannic acid (TA–COOH) was first prepared through a simple esterification between TA and methylhexahydrophthalic anhydr...

The influence of surface modifications on the mechanical properties of epoxy-hexagonal boron nitride nanoflake (BNNF) nanocomposites is investigated. Homogeneous distributions of boron nitride nanoflakes in a polymer matrix, preserving intrinsic material properties of boron nitride nanoflakes, is the key to successful composite applications. Here, a method is suggested to obtain noncovalently f...

The fracture toughness and uniaxial tensile yield strengths of unmodified and CTBN-rubbermodified epoxies were measured under hydrostatic pressure. The purpose of these experiments was to learn how suppressing cavitation in rubber particles affects the deformation mechanisms and the fracture toughness of rubber-modified epoxy. It was found that the cavitation of CTBN-rubber could be suppressed ...

Novel self-repairing Urea-Phenol-Formaldehyde (UPF) microcapsules containing linseed oil were prepared via in-situ polymerization in an oil-in-water emulsion. The main purpose of encapsulation is to control the release of linseed oil, when external conditions such as mechanical stress or energy cause microcapsules to break. These controlled release mechanisms of linseed oil make them suitable f...

The sol-gel technique was used to prepare epoxy/silica nano-hybrids. The thermal characteristics, curing kinetics and structure of epoxy/silica nano-hybrids were studied using differential scanning calorimetry (DSC), 29Si nuclear magnetic resonance (NMR) and transmission electron microscopy (TEM). To improve the compatibility between the organic and inorganic phases, a coupling agent was used t...

Concrete-epoxy interface can be found in many strengthened or retrofitted structures, especially in Hong Kong where concrete structures are the majority. In practice, epoxy is usually used in repairing concrete structures because of its excellent adhesion, chemical and heat resistance, good mechanical properties and electrical insulating properties. The bond between concrete and epoxy has been ...

Functionalization of single-walled carbon nanotubes (SWNTs) with covalently grafted amine moieties provides reactive fillers with potential covalent anchoring to an epoxy matrix. Manufacturing and characterization of a high performance epoxy system reinforced with as-grown and aminated SWNTs are presented through four different approaches. Epoxy composite materials incorporating SWNTs aminated ...

Wood is one of the earliest and most common building materials on the planet. However wood also quickly decays under normal service conditions, and thus the repair of historic structural elements pose a difficult challenge to preservation professionals who aim to also preserve the authenticity of the element. Since the 1970s, numerous studies have looked at the use of epoxy with respect to hist...