Dispersive liquid-liquid microextraction (DLLME) followed by gas chromatography-massspectroscopy (GC-MS) was used to analyses of components of floral-water of Rosmarinusofficinalis . Some effective parameters such as volume of extraction, disperser solvents andsalt effect were studied by a full factorial design for obtain the optimum condition. The maincompounds of the floral-water of Rosmarinu...

The techniques and measurement methods developed in the Environmental Survey and Monitoring of Chemicals by Japan's Ministry of the Environment, as well as a large amount of knowledge archived in the survey, have led to the advancement of environmental analysis. Recently, technologies such as non-target liquid chromatography/high resolution mass spectrometry and liquid chromatography with micro...

Extraction and determination of naproxen from human plasma were performed using Vortex-Assisted Inverted Dispersive Liquid-Liquid MicroExtraction (VA−IDLLME) and High-Performance Liquid Chromatography (HPLC). The parameters affecting extraction recovery such as type and volume of extraction and disperser solvents, pH of sample solution, stirring rate, extraction time and salt addition were ...

Liquid chromatography is a widely popular technique in clinical laboratories and clinical applications. People evolved and developed various types of chromatography for decades after its initial idea published in 1960s. Mostly people use HPLC-MS, UHPLC techniques to purify antibody, drug isomers and enantiomers. Separating molecules of different sizes by modified HPLC and size exclusion chromat...

Dispersive liquid-liquid microextraction method (DLLME) combined with high-performance liquid chromatography-ultraviolet detection (HPLC-UV) was used to determine thiamine (B1), nicotinamide (B3) and pyridoxine (B6) in sour cherry juice. This method was rapid, simple and sensitive. Separation was accomplished using a C18 column. The optimum chromatographic conditions were found to be: mobile ph...

Supercritical fluid and microbore liquid chromatography offer potential applications for drug analysis. In supercritical fluid chromatography (SFC), the mobile phase is a gas (e.g., carbon dioxide) maintained at its supercritical state--that is, above its critical temperature and pressure, above which it cannot be liquefied even with further increases in applied pressure. The SFC mobile phase h...

Garrido JL and Zapata M (1996) Ion-pair reversed-phase high-performance liquid chromatography of algal chlorophylls. Journal of Chromatography A 738: 285. Hodgson DA, Wright SW and Davies N (1997) Mass spectrometry and reverse phase HPLC techniques for the identiRcation of degraded fossil pigments in lake sediments and their application in palaeolimnology. Journal of Paleolimnology 18: 335. Jef...

Propolis is a natural resin of a variety of plant origins collected by honeybees to seal gaps and cracks in their hives. Propolis was used as a remedy of various diseases due to its versatile biological activities. At least 200 compounds have been identified in the world. The present study aimed to investigate the chemical composition of two samples of Sudanese propolis collected from El-Faki H...