Coherent X-ray diffraction is a useful technique for understanding the structure of compact objects including those which can be represented as phase objects. X-rays are highly penetrating and have wavelengths very close to atomic spacing. In this work, gold nanocrystals (on a reflecting substrate) were imaged at the Advanced Photon Source and found to produce a novel double diffraction pattern...

biocl microflowers were synthesized using bismuth nitrate pentahydrate and sodium chloride by microwave (mw) assisted synthesis method for 23 minutes at 180 w. scanning electron microscopy (sem) studies revealed a unique morphology of flower-like assemblies comprised of nanosheets. the x-ray diffraction (xrd) pattern showed that a highly pure and crystalline phase has been obtained. the energy ...

the monolithic oxynitride glasses in sio2-al2o3-b2o3 system were synthesized using sol-gel method. the porous, dried gels were heated in flowing ammonia for different times and varying temperatures. the nitrogen content of the oxynitride glasses was determined using an oxygen-nitrogen analyzer. the chemical bonding state and properties of glasses were investigated by means of fourier transform ...

Degradation or polyethylene glycol has been studi ed by UV irradiation. A drastic change in the morphology from spherulite to rhythmic pattern has been observed under polarized light microscope when exposed to UV light. Molecular weight of PEG. Rr value and melting point have been recorded after UV exposure. On UV exposure there has also been a change in UV. IR and powder X-ray diffraction patt...

Figure S1. Rietveld refinement patterns of PCN-888 using synchrotron PXRD data (λ = 0.72768Å): observed (blue), calculated (red), and difference (grey) profiles are shown; the tick marks below the curves indicate Bragg positions. The X-ray diffraction pattern between 1.1° and 4.2° is magnified in the inset. The full pattern shows a precise match between the experimental PXRD data and those simu...

Graphene-based nanocomposites are newly emerged materials with a wide range of applications such as in supercapacitors electrode. The high conductivity and ability for passing electric current, makes Graphene an appropriate new item to be used in cells. Electroactive transition metal oxides, owing fast reversible redox pairs, are used to store electrical charge. Furthermore, the Graphene/NiO na...

superparamagnetic single phase zinc ferrite nanoparticles have been prepared by coprecipitation method at 20 °c without any subsequent calcination. the composition, crystallite size, microstructure and magnetic properties of the prepared nanoparticles were investigated using x-ray diffraction (xrd), field emission scanning electron microscope (fesem), transmission electron microscope (tem), fou...

we report the growth by ion exchange synthesis of zns nanoparticles in mcm-41 matrices using zn (ch3coo)2 and na2s starting sources. the final product (zns/mcm-41) was characterized by x-ray diffraction (xrd) pattern, transmission electron microscopy (tem), scanning electron microscopy (sem), infrared spectrometry (ir) and uv-vis spectroscopy. its crystalline structure and morphology was studie...

According to circumstance of kerman sarcheshmeh cooper complex that its anode slime is mainly consisted of Cu, Ag, Au, Pb and Se. In this work, recovery of silver from anode slime and subsequent synthesis of silver nanoparticles from leaching solution was made. Silver was separated from anode slime by using of HNO3 and HCl. X-Ray fluorescence spectroscopy (XRF) was used to characterize anode sl...

According to circumstance of kerman sarcheshmeh cooper complex that its anode slime is mainly consisted of Cu, Ag, Au, Pb and Se. In this work, recovery of silver from anode slime and subsequent synthesis of silver nanoparticles from leaching solution was made. Silver was separated from anode slime by using of HNO3 and HCl. X-Ray fluorescence spectroscopy (XRF) was used to characterize anode sl...