نتایج جستجو برای: thermo mechanical processing x ray diffraction analysis
تعداد نتایج: 3922480 فیلتر نتایج به سال:
In this paper, the bismuth vanadate (BiVO4) nanoparticles were synthesized at 600 °C calcination temperature by co-precipitation method. To study the crystal structure, morphology, optical and photocatalytic properties of the samples, the X-ray diffraction analysis, field emission scanning electron microscopy, energy-dispersive X-ray spectroscopy, Fourier-transform infrared spectroscopy and ult...
Introduction Individual X-Ray diffraction patterns of biological tissues are obtained via interference of coherent scattering with their electrons. Many scientists have distinguished normal and cancerous breast tissue, bone density, and urinary stone types using the X-Ray diffraction patterns resulting from coherent scattering. The goal of this study was to introduce an optimized method for obt...
The synthesis of AlN and TiB2 by spark plasma sintering (SPS) and the effect of Nb2O5, Y2O3 and ZrO2 additions on the mechanical properties and densification of the produced composites is reported and discussed. After the SPS process, dense AlN and TiB2 composites with Nb2O5, Y2O3 and ZrO2 were successfully prepared. X-ray diffraction analysis showed that in the AlN composites, the addition of ...
Two copper complexes, Cu(SCN)(Mpz(∗)T-(EtO)2) (1) (Mpz(∗)T-(EtO)2=L3) and CuCl(H2O)(Mpz(∗)T-O2) (2) (Mpz(∗)T-O2=L4) were synthesized by the reaction of 2,4,6-tri(3,5-dimethylpyrazol-1-yl)-1,3,5-triazine (L1) or 2,4,6-tri(1H-pyrazol-1-yl)-1,3,5-triazine (L2) with CuCl2·2H2O in anhydrous ethanol and methanol, respectively. The complexes were characterized by elemental analysis, IR spectroscopy, t...
In the present research, to form niobium carbide coating on the surface of AISI L2 steel Thermo-Reactive Deposition method (TRD) in a molten bath was used. Niobium carbide coating treatment was carried out at 1173 K, 1273 K, and 1373 K for 2, 4, and 8 hours. The molten bath contained 20wt.% borax (Na2B4O7), 5 wt.% boric acid (B2O3), and 75 wt.% ferro-niobium. The presence and properties of...
A novel sulfonated polybenzimidazole/organoclay (Cloisite-30B) (SPBI/clay) nanocomposite membranes was successfully synthesized based on aromatic diacide (1) and diaminobenzidine. Nanocomposite membranes were fabricated using 1, 4-bis (hydroxymethyl) benzene (BHMB) as cross-linker, and Cloisite-30B organoclay as the pseudo cross-linker. The cross-linked SPBI/clay nanocomposite membranes were pr...
Urinary calculi constitute one of the oldest afflictions of humans as well as animals, which are occurring globally. The calculi vary in shape, size and composition, which influence their clinical course. They are usually of the mixed-type with varying percentages of the ingredients. In medical management of urinary calculi, either the nature of calculi is to be known or the exact composition o...
The typical as-built coarse and cube-oriented microstructure of Inconel® 625 parts fabricated via arc-based directed energy deposition (DED) induces anisotropic mechanical behavior, reducing the potential applications DEDed in critical components. In this sense, present work aimed to reduce grain size texture by applying an situ interlayer hot forging (HF) combined with post-deposition heat tre...
In this work, copper oxide nanoparticles have been synthesized via extractive Rosmarinus Officinalis leaves by simple and economic co-precipitation method at ambient conditions which it has used (CH3COO)2Cu+H2O individually as Cu sources. It was found that uniform copper oxide nanoparticles have been successfully produced at various temperature, namely 400, 600, and 800 0C. Powder X-ray Diffrac...
In this study, a kind of Ni-based superalloy specially designed for additive manufacturing (AM) was investigated. Thermo-Calc simulation and differential scanning calorimetry (DSC) analysis were used to determine phases their transformation temperature. Experimental specimens prepared by laser metal deposition (LMD) traditional casting method. Microstructure, phase constitution mechanical prope...
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