In the current work the kinetics of dehydration of ziprasidone hydrochloride monohydrate was studied by nonisothermal thermogravimetry. Ziprasidone hydrochloride monohydrate was heated from 30 to 150° with a heating rate of 5° per min under nitrogen gas atmosphere and weight loss data were collected. Powder X-ray difraction was used to characterize the solid before and after dehydration. The we...

The polyamine (PA) was prepared by condensation of 1,4-bischloromethyl benzene and benzidine. The PA was then treated with cyanuric chloride at 0°C followed by reaction with 5-amino-8-Hydroxyquinoline in THF in conc. NaOH (PH 9-10) at room temperature for 8 hrs. The resultant polymer designated as polyamine-s-triazine-5-amino8-Hydroxyquinoline (PATHQ) was characterized by elemental analysis, IR...

In the last decade, adsorption has been used to minimize the pollution caused by dyes, which represents a serious environmental problem. In this context, this work reports the preparation of phthalic anhydride-modified cellulose (PhCel), through the reaction of cellulose (Cel) with phthalic anhydride (Ph). The efficiency of the reaction was observed by elemental analysis, Fourier Transform Infr...

In this paper we elected to nitrate p-xylene because this compound has only one mononitro- and trinitro- isomer. Trinitro-p-xylene was used as a starting material for the synthesis of other compounds in subsequent work. The mononitration of p-xylene can be easily carried out at 30 degrees C. Nitro-p-xylene is easily nitrated to dinitro-p-xylene at a temperature of 80 degrees C. The trinitro-p-x...

The aim of this study is to prepare a solid fuel from the most abundant biomass of Morocco that can be used by the local population, and in particular by the rural ones, instead of the wood of forest, which is less available and its exploitation is negative for the environment. Esparto is the most available biomass, with a production of 560000 tons annually of dry matter approximately. However,...

Abstract Studies on original mortars can greatly assist archaeological interpretations, as elucidating the composition of such gives clues origin raw materials, manufacturing technology, and construction phases a site. This article presents multi-analytical characterisation 24 plasters from Żejtun Roman Villa, Malta, to support hypotheses history The samples, belonging at least three distinct i...

Objective This study evaluated alterations in cortical morphology in patients with transient global amnesia (TGA). Materials and Methods Diagnoses of TGA occurred at our hospital. Evaluation involved a structured interview to obtain clinical information and a brain magnetic resonance imaging scan. We analyzed whole-brain T1-weighted MRI data using FreeSurfer 5.1. Measures of cortical morpholo...

PURPOSE Transient global amnesia (TGA) is a syndrome of unknown etiology. Electroencephalographic (EEG) abnormalities in TGA have been reported previously. We analyzed the frequency and characteristics of EEG abnormalities in patients with TGA. METHODS We collected EEGs of patients with a clinical diagnosis of TGA who had visited the emergency room or the outpatient clinic over a period of 8 ...