نتایج جستجو برای: transmission electron microscope tem

تعداد نتایج: 567607  

Journal: :Microscopy and Microanalysis 2023

Current progress in programmable electrostatic phase plates raises questions about their usefulness for specific applications. Here, we explore different designs such with the goal of correcting spherical aberration Transmission Electron Microscope (TEM). We numerically investigate whether a plate could provide down to 1 $\r{A}$ngstr\"om spatial resolution on conventional uncorrected TEM. Diffe...

2007
A. Genç D. P. Basile G. B. Viswanathan

Despite the significant advances in the transmission electron microscope (TEM), such as application of aberration correction and monochromation [1], sample preparation is still one of the most critical steps determining the quality, and precision of the results. The important challenge here is to prepare samples that are thin enough for electron transparency, free from any surface damage and al...

Journal: :iranian journal of hydrogen & fuel cell 2014
ashkan esmaeilifar soosan rowshanzamir amin behbahani

a hydrothermal method for preparation of nano-size zirconia has been studied to optimize the effective parameters (precursor concentration, temperature and time) using response surface methodology (rsm). the synthesized zirconia samples were characterized through x-ray diffraction (xrd), scanning electron microscope (sem) and transmission electron microscopy (tem) analyses to identify mean nano...

Journal: :Journal of colloid and interface science 2008
Marek S Zbik Ray L Frost Yen-Fang Song Yi-Ming Chen Jian-Hua Chen

The utilization of new transmission X-ray microscopy (TXM) using the synchrotron photon source enable for the first time the study in three dimensions microsize clay particles in aggregates in their natural aqueous environment. This technique makes possible remarkable accurate images of nanosize mineral interparticle structure which forms a new nanocomposite. The Birdwood kaolinite/LDH aggregat...

2015
B. Gowramma U. Keerthi Mokula Rafi D. Muralidhara Rao

In the present study, synthesis, characterization, and the antibacterial activity of silver nanoparticles from native isolate of Corynebacterium glutamicum has been reported. Silver nanoparticles were synthesized by challenging the dried biomass of C. glutamicum with aqueous diamine silver ([Ag (NH3)2]+) containing 1 mM AgNO3. Synthesized silver nanoparticles (AgNPs) were characterized by ultra...

2009
Enrico Mugnaioli giancarlo capitani FErnando niEto MarcEllo MEllini

Lattice parameters for gold nanocrystals, quartz, and vesuvianite have been determined by electron diffraction in routine transmission electron microscopy (TEM) work, with precision and accuracy near to 0.1%, after correction for elliptical distortion. The distortion, measured in three different microscopes, is constant for each microscope and may be easily eliminated. Variable camera constants...

Journal: :Ultramicroscopy 2011
U Kaiser J Biskupek J C Meyer J Leschner L Lechner H Rose M Stöger-Pollach A N Khlobystov P Hartel H Müller M Haider S Eyhusen G Benner

The electron optical performance of a transmission electron microscope (TEM) is characterized for direct spatial imaging and spectroscopy using electrons with energies as low as 20 keV. The highly stable instrument is equipped with an electrostatic monochromator and a C(S)-corrector. At 20 kV it shows high image contrast even for single-layer graphene with a lattice transfer of 213 pm (tilted i...

Journal: :organic chemistry research 0
sobhan rezayati islamic azad university zahra abbasi chemistry department, college of science shahid chamran university, ahvaz, iran eshagh rezaee nezhad department of chemistry, payame noor university, po box 19395-4697 tehran, iran rahimeh hajinasiri chemistry department, qaemshahr branch, islamic azad university, p.o. box 163, qaemshahr, iran shahin soleymani chalanchi 1department of chemistry, payame noor university, po box 19395-4697 tehran, iran

a simple and facile method for the preparation offe2+ supported on hydroxyapatite-core-shell-γ-fe2o3 nanoparticles (γ-fe2o3@hap-fe2+ nps) as an environmentally friendly and recyclable green catalyst is described and used for the one-pot synthesis of benzimidazoles and benzoxazole derivatives via reactions between aromatic aldehydes and ortho‐phenylenediamine or ortho‐aminophenol in aqueous medi...

2013
Cenap Ozkara

Objectives: As we known that the internal thoracic artery (ITA) has an excellent patency rate in coronary artery bypass grafting (CABG). However, early graft failure due to occlusion and spasm is still the major problem after coronary artery bypass surgery. We examined histopathologic findings of the clipped internal thoracic artery (ITA) in patients undergoing CABG using transmission electron ...

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