نتایج جستجو برای: accelerated solvent extraction

تعداد نتایج: 273883  

Journal: :Molecules 2014
Yuan-Feng Zou Bing-Zhao Zhang Hilde Barsett Kari Tvete Inngjerdingen Drissa Diallo Terje Einar Michaelsen Berit Smestad Paulsen

The root bark, stem bark and leaves of Terminalia macroptera were sequentially extracted with ethanol, 50% ethanol-water, and 50 °C and 100 °C water using an accelerated solvent extractor. Ten bioactive purified polysaccharide fractions were obtained from those crude extracts after anion exchange chromatography and gel filtration. The polysaccharides and their native extracts were characterized...

Abdi, Khosrou , Daneyali, Ali , Heidari, Mahmoud , Heravizadeh, Omid , Kamgou, Somayeh , Khadem, Monire , shahtaheri, Seyed Jamaloddin ,

Introduction: Todays, exposure to heavy metals is happened by being produced in various environmental, industrial processes. The production of metals finally results in air pollution as well as contamination in the food chain. There are harmful effects of heavy metals such as cadmium on different organs. Therefore, this study aimed to identify and quantify cadmium in biological samples using DL...

Journal: :Journal of chromatography. A 2015
Runzeng Liu Ting Ruan Shanjun Song Yongfeng Lin Guibin Jiang

Robust analytical methods were developed for the determination of eight emerging synthetic phenolic antioxidants (SPAs) and three metabolites in sewage sludge, effluent and river water matrices. Accelerated solvent extraction was employed for the extraction of the target analytes from sludge, dichloromethane/hexane=3:1 (extraction solvent) and 90°C (extraction temperature) were used after optim...

2010
Elin Löfström-Engdahl Emma Aneheim Christian Ekberg Mark Foreman

The fact that the choice of organic diluent is important for a solvent extraction process goes without saying. Several factors, such as e.g. price, flash point, viscosity, polarity etc. each have their place in the planning of a solvent extraction system. This high number of variables makes the lack of compilations concerning diluent effects to an interesting topic. Often the interest for the r...

Journal: :Talanta 1969
T Fujinaga T Kuwamoto E Nakayama

A low-melting solid is used as organic solvent for liquid-liquid extraction at elevated temperatures followed by solidification and decantation of the aqueous phase.

Precious metals are currently associated with selenium (naumannite, Ag2Se) and tellurium (calaverite, AuTe2; sylvanite, (Au,Ag)2Te4) to form species refractory to cyanidation. The aim of this preliminary work was to study the use of the solvent extraction technique to recover tellurium and selenium ions from a synthetic solution similar to the cyanidation effluents to recycle the free cyanide b...

Journal: :Journal of chromatography. A 2003
M Ramil Criado I Rodríguez Pereiro R Cela Torrijos

An alternative method for the extraction of polychlorinated biphenyls (PCBs) in ash samples, which is less time and solvent consuming than Soxhlet extraction, is presented. A study was carried out to evaluate the possibilities of microwave-assisted extraction (MAE) to determine exactly which parameters affect the efficiency of the process, since direct extrapolation of extraction conditions for...

2009
Zurina Zainal Abidin Sepidar Sayyar Robiah Yunus

Problem statement: Jatropha curcas is a wonder plant with a variety of applications and enormous economic potentials. Oil from the seeds can be used as alternative fuel and for making biodiesel which aims to overcome energy crisis problems. In this study, extraction of Jatropha oil from seeds was optimized using organic solvent based on the amount of the extracted oil. The kinetics of extractio...

Journal: :Food technology and biotechnology 2017
Hasene Keskin Çavdar Derya Koçak Yanık Uğur Gök Fahrettin Göğüş

Pomegranate seed oil was extracted in a closed-vessel high-pressure microwave system. The characteristics of the obtained oil, such as fatty acid composition, free fatty acidity, total phenolic content, antioxidant activity and colour, were compared to those of the oil obtained by cold solvent extraction. Response surface methodology was applied to optimise extraction conditions: power (176-300...

Masoumeh Hemmati Mohammad Reza Hajmohammadi,

Extraction and determination of naproxen from human plasma were performed using Vortex-Assisted Inverted Dispersive Liquid-Liquid MicroExtraction (VA−IDLLME) and High-Performance Liquid Chromatography (HPLC). The parameters affecting extraction recovery such as type and volume of extraction and disperser solvents, pH of sample solution, stirring rate, extraction time and salt addition were ...

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