a simple method has been developed for the preconcentration of lead (ii) based on the adsorption of its 1-(2-pyridyl azo)2-naphtol (pan) complex on aoctadecyl bonded silica cartridges. the influence of acidity, eluting agents, stability of the column, sample volume and interfering ions has been investigated in detail. the adsorbed complex could be eluted using environmentally benign hno34m and ...

A simple, rapid and efficient dispersive liquid–liquid microextraction by use of ionic liquid (IL-DLLME)method, followed by flame atomic absorption spectrometry (FAAS) was developed for the preconcentrationand determination of palladium in water samples. In this method, an appropriate mixture of acetone and octylmethyl imidazolium hexafluorophosphate was injected rapidly into the aqueous sample...

Pb and Cd in water samples were determined by cloud point extraction (CPE) with sodiumdiethyldithiocarbamate (DDTC) as the chelating agent and octylphenoxypolyethanl (Triton X-114) asthe surfactant prior to flame atomic absorption spectrometry (FAAS) determination. The main factorsof affecting the extraction and detection processes were optimized. The preconcentration of 10 mL ofstandard soluti...

Extensive distribution of hazardous substances in food chain and the deleterious effect of their residues on public health are a great concern of the society. Chicken eggs, as one of the most popular food commodities, in different parts of Tehran (Iran) were analyzed for two groups of hazardous substances including some organochlorine pesticides (OC) such as aldrin, lindane, dieldrin, dichlorod...