Anisole is a straw-colored aromatic compound mainly used in making solvents, flavoring agents, perfumes, fuel additives, and the synthesis industries. Anisole, also known as methoxybenzene, synthesized from sodium phenoxide or phenol using various methylating agents. The use of dimethyl ether (DME) an alkylating agent seldom reported literature. Herein, we have anisole through O-alkylation proc...